GCMS analysis report for sample AE01511, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report •’ Data File : C:\MSDCHEM\l\5973N\02FEB21\01511 .D Vial: 2 Acq On : 21 Feb 2002 4:01 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 1-METHOXYMETHOXY-1,4-CYCLOH... Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 13.38 0.04 ug/L 26029 Naphthalene-d8 13.20 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 1-METHOXYMETHOXY -1,4-CYCLOHEXADI... 140 C8H12O2 057234-30-7 5 2 Dicyclopropylmethanimine, N-cyano- 134 C8H10N2 000000-00-0 5 3 Benzene, (2-propenyloxy)- $$ Eth... 134 C9H10O 001746-13-0 4 4 2-Methyl-3-methoxy-4H-pyran-4-one 140 C7H8O3 000000-00-0 4 Abundance Scan 886 (13.376 min): 01511.D (-) m/z 140.00 100.00% 140

5000

94

m/z—> 49 I 8 I ' 1 1 1 1 1 1 ‘I • 30 40 50 66 I 1 11*11141111* 60 70 80 84... * 108 90 ' 1 I ' ‘ ‘ ‘ I ‘ 100 110 120 130 140 134 -4 13.00 13.20 13.40 13.60 13.80 m/z 94.00 15.16% Abundance #35609:1-METHOXYMETHOXY-1.4-CYCLOHEXAD1ENE $$ 1,4-Cyclohe... 45

. j ... f | \ I I 1^' I ! 1 1 | I I I . | 1 ' 5000 13.00 13.20 13.40 13.60 13.80 m/z66.00 13.79% 67 77 _ 95 ... 110 140 । 0 f"r* 1 1 i ‘4 — ■ । i Pi i'| . i i । । । n ( । । i i i I । i > । /z—> 30 40 50 60 70 80 90I 100 110 120 130 140 Abundance #29457: Dicyclopropylmethanimine, N-cyano- 41

13.00 13.20 13.40 13.60 13.80 5000 93 133 m/z 134.10 13.63% 79 106 66 119

/z—> 0- i ■ ‘ ■ 1 i ■ ■ ‘ ■ i • ■ ■ ■ i ■ ■ 30 40 50 60 70 80 pl1..... 1, ' ’ 1 J । 1 ' I 1 1 90 100 110 120 130 140 Abundance #29590: Benzene, (2-propenyloxy)- $$ Ether, allyl phenyl $... 41 13.00 13.20 13.40 13.60 13.80 m/z 70.00 11.21%

5000 134 65 94 77 119

m/z—> 0 I 1 1 ' 1 1 1 1 TPPT I**‘I** 30 40 50 60 70 80 90 I 100 110 120 । . 130 t ‘ * I IiI 140 .... A....... 1 13.00 13.20 13.40 13.60 13.80

31511.D HP022102.M Mon Feb 25 10:55:17 2002 Page 8

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