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GCMS analysis report for sample AE01511, March 2002

Machine-extracted title · confidence 100%

GCMS laboratory results for sample AE01511 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.

NYC-WTC_000010047–000010065

Folder label: “GCMS X 1/23/02 A 2/21/02”

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Scanned page image, NYC-WTC_000010059
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB21\01511.D Vial: 2 Acq On : 21 Feb 2002 4:01 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 3-Hydroxy-2,2,4-trimethyl-3... Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

16.55 0.02 ug/L 15345 Acenapht hene-d10 18.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

l 3-Hydroxy-2,2,4-trimethyl-3-pent... 140 C8H12O2 003173-79-3 5 2 4-Isopropylcyclohexanone $$ Cycl... 140 C9H160 005432-85-9 5 3 2H-Pyran-5-carboxylic acid, 2-ox... 140 C6H404 000500-05-0 5 4 3-Methoxy-2-methyl-cyclohex-2-enone 140 C8H12O2 025112-91-8 5 Abundance Scan 1167 (16.548 min): 01511 .D (-) m/z 140.10 100.00% 140

5000 122 84 172 71 16.20 16.40 16.60 16.80 0 1 I“' 'I‘ ‘ ' I • ‘ ‘' I ‘‘ ' I ' 1 ' ‘ I ' ‘ ' I' I | l I n frr.. | . . . , | *‘1** ‘ 1’111111111 TTp m/z 122.00 35.49% miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #35758:3-Hydroxy-2,2,4-trimethyl-3-pentenoic acid .beta.-... 70 42 5000- 81 140 16.20 16.40 16.60 16.80 m/z 172.20 28.48% 27 96 I - 0- ■ i ■ ■ ■ ■ i ■ ■ ■' i ■i " i' ■•। • i • • > • j»• > • i ■ iz-> :20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #36265:4-Isopropyicyclohexanone $$ Cyclohexanone, 4-(1-me... 43 69 140 55 84 16.20 16.40 16.60 16.80 5000 m/z 136.10 26.02% 97 107 122

0' ■ i “ “ i ■ “ ■ i11 ‘11 “ ‘11 ‘“ i “ " i ■ 111 ■ “ i •' • i" •' “ I ' " 1 I 'Till i n ip niz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #35121: 2H-Pyran-5-carboxylic acid, 2-oxo- $$ .alpha.-Pyro... ■ ■ i ' ■ 1 1 i ' ■ ' ' i ■ ■ i ‘ ■ i 1 39 112 16.20 16.40 16.60 16.80 140 m/ Z 84.00 23.53%

5000 J M v/ ABN L A Ml 66 84 123

m/z—> O‘i 11 “ 11 “ T H49 * i *' * • F 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 IIBBatITmm 1’1’001—01370 FI ‘ * i * • ‘ 1 1 ‘ * 16.20 16.40 16.60 16.80

01511.D HP022102.M Mon Feb 25 10:55:17 2002 Page 9

NYC-WTC_000010059

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NYC-WTC_000010059Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.998

machine-extracted · confidence unavailable · Check page ↗
DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004935

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.998

machine-extracted · confidence unavailable · Check page ↗

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