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GCMS analysis results for sample AD29522, Feb 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AD29522 listing unknown compounds and surrogate recovery data from February 8, 2002.

NYC-WTC_000036779–000036797

Folder label: “GCMS X 12/7/01 A 1/2/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB01\29522.D vial: 4 Acq On : 1 Feb 2002 1:04 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 2H-Pyran, tetrahydro-2-[(te... Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 19.97 0.04 ug/L 24655 Acenaphthene-dl0 18.34 Hit# of 5 Tentative ID MW MolForm CAS# Qual 180 1 2H-Pyran, tetrahydro-2- [(tetrahy... 186 C10H18O3 000710-14-5 9 ~9 2 1,2-Cyclohexanediol, l-methyl-4- ... 172 C10H20O2 033669-76-0 90 . 3 Butanoic acid, 2-ethylhexyl ester 200 C12H24O2 oooooo-oo-o 9 4 Imidazole-2,4,5-d3 $$ lH-Imidazo... 71 C3HD3N2 006745-43-3 4 Abundance Scan 1454 (19.974 min): 29522.D (-) m/z 71.10 100.00% 71

5000

43 56 83 185 N 19.60 19.80 20.00 20.20 20.40 O-mpmmm 1—0100000000 -rp-r m/z 185.10 20.94% miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #95189: 2H-Pyran, tetrahydro-2-[(tetrahydro-2-furanyi)meth... 71 55

5000 27 84 • i • ' ■ ■ i ■ ■ • • i 1 i • ‘ • i ■ 19.60 19.80 20.00 20.20 20.40 42 m/z 186.10 19.57%

miz-> O-p H pmmmmmmmmmmmmmmmmmmmp 20 30 40 SO 60 70 80 80 100 110 120 130 140 150 160 170 180 190 Abundance #76524:1,2-Cyclohexanediol, 1 -methyl-4-(1 -methylethyl)- $... 71

19.60 19.80 20.00 20.20 20.40 5000- m/z 56.10 18.46% 111 58 83 ! 97 129 139 172 O-pmppt -p-rrrp-r - IImhmmp mppm m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #115444: Butanoic acid, 2-ethylhexyl ester ■ I ‘ ‘ 1 ‘ ' 1 1 ■ ‘ 1 I 11 1 1 T 43 71 19.60 19.80 20.00 20.20 20.40 m/z 49.00 17.93% 5000 55 AwW A M A WANANs 112 102 | 0- ■ i" ■ ‘i1" ■ i “ ■ i ■ ■ 11 ■ ■ 1 TT I 11 (u 111111 111! Ij 11 I n 1, 11 n I ||| n । : 4 i ■ ‘ 1 1 i ■ miz—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 19.60 19.80 20.00 20.20 20.40

29522.D SCAN508.M Mon Feb 04 08:41:12 2002 Page 11

NYC-WTC_000036793

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NYC-WTC_000036793Source: NYC Law Department, mirrored locally

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