Laboratory report documenting gas chromatography-mass spectrometry results for sample AE03075 including surrogate recovery.
NYC-WTC_000010927–000010946Folder label: “GCMS X 2/5/02 A 2/28/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
• Data File : C:\MSDCHEM\l\5973N\02FEB28\02716 .D Vial: 1 Acq On : 28 Feb 2002 2:40 pm Operator: Sample . : 508 scan Inst : Instrumen Mise : February 28, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 3-Hydroxy-2,2,4-trimethyl-3... Concentration Rank 12
R.T. EstConc Area Relative to ISTD R.T.
16.55 0.04 ug/L 21076 Acenaphthene-dl0 18.33
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Hydroxy-2,2,4-trimethyl-3-pent... 140 C8H12O2 003173-79-3 5 2 2H-Pyran-5-carboxylic acid, 2-ox... 140 C6H404 000500-05-0 5 3 Pyrazine, 2-methyl-3-(methylthio... 140 C6H8N2S 002882-20-4 5 4 1,3-Cyclopentanedione, 2-acetyl-... 140 C7H803 003859-39-0 5 Abundance Scan 1167 (16.548 min): 02716.D (-) m/z 140.10 100.00% 140
5000 172 84 122 71 T T i TI It 16.20 16.40 16.60 16.80 oV ■ i ‘ ■ i ■ ■ ■' i1 ■ ‘ ■ i ■'111 ■ i ■ *'111' • ■ i • ■ ■ • i ■ ■ i ‘ ■ i1 ■ ■ ■ i TT-p m/z 172.20 36.66% nz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #35758:3-Hydroxy-2,2,4-tnmethyl-3-pentenoic acid .beta.-... 70 42
5000 0 81 140 16.20 16.40 16.60 16.80 m/z 122.10 25.65% 27 96 I ,, I. I 0•i■“■i■■■■i ■ ■ i ■ • ‘ • i > > h1i > I i i । reh—H i i i । i i . i । i i " i ■ ■ " i " " i • " ■ i1 n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #35121: 2H-Pyran-5-carboxylic acid, 2-oxo- $$ .alpha.-Pyro... 39 112 140 16.20 16.40 16.60 16.80 1 ‘ 5000 m/z 83.90 23.98% 66 84
8111111111 118 • 11 • •»■ j 11 49 1 l •“ 'I ' 123
■' ।1 • ■1111 “I""I"‘1i11"11 AA kNAnM w A fJ
-n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #35175: Pyrazine, 2-methyl-3-(methylthio)- (CAS) $$ 2-Meth... 140 16.20 16.40 16.60 16.80 4 m/z 138.1023.11% 5000 107 42 125 66 84 94 — .............. .. ........... 01, | 1 4 >. | 1 ■. ■ | ■ i ■ i • • * ‘ i11 ‘ l' “ • l ‘ -mpp —mmmmmmp m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 16.20 16.40 16.60 16.80
02716.D HP022102.M Fri Mar 01 10:07:15 2002 Page 10
NYC-WTC_000010940
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NYC-WTC_000010907
Laboratory report documenting gas chromatography-mass spectrometry results for sample AE03075 including surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011007
Laboratory report documenting gas chromatography-mass spectrometry results for sample AE02721 including surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010106
GCMS laboratory results for sample AE01637 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010867
Laboratory report documenting gas chromatography-mass spectrometry results for sample AE02713 including surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010947
Laboratory report documenting gas chromatography-mass spectrometry results for sample AE03075 including surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010066
GCMS laboratory results for sample AE01547 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009966
Analytical results for sample AE01508 analyzed via GCMS on March 4, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010027
GCMS laboratory results for sample AE01510 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010887
Laboratory report documenting gas chromatography-mass spectrometry results for sample AE03075 including surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010047
GCMS laboratory results for sample AE01511 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000004494
Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000004935
Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000010837
Administrative record from DEP Box 14 covering the period of February to March 2002 regarding World Trade Center environmental activities.
Filed in the same folder
NYC-WTC_000010838
Technical log recording laboratory parameters and counts for sample AE02713 processed in late February 2002.
Filed in the same folder
NYC-WTC_000010843
Laboratory report documenting a blank run for gas chromatography-mass spectrometry analysis of sample AE02713.
Filed in the same folder
NYC-WTC_000010862
Laboratory report documenting a reference standard run for gas chromatography-mass spectrometry analysis of sample AE02713.
Filed in the same folder
NYC-WTC_000010867
Laboratory report documenting gas chromatography-mass spectrometry results for sample AE02713 including surrogate recovery.
Filed in the same folder