GCMS analysis results, Feb 27 2002

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Laboratory report showing GC/MS analysis results for sample AE01136 testing unknown compounds and specific analytes on February 27, 2002.

NYC-WTC_000003444–000003462

Folder label: “GCMS X 1/20/02 A 2/25/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB25\01136.D vial: 3 Acq On : 25 Feb 2002 12 :53 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 2H-Pyran-5-carboxylic acid,... Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

16.55 0.04 ug/L 23269 Acenaphthene-dl0 18.33

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2H-Pyran-5-carboxylic acid, 2-ox... 140 C6H404 000500-05-0 9 2 1,3,5,7-Tetraazatricyclo [3.3.1.1... 140 C6H12N4 000100-97-0 7 3 1,3-Cyclopentanedione, 2-acetyl-... 140 C7H803 003859-39-0 5 4 Methylphloroglucinol 140 C7H803 000000-00-0 5 Abundance Scan 1167 (16.548 min): 01136.D (-) m/z 140.10 100.00% 140

5000 172 44 122 84 16.20 16.40 16.60 16.80 0 • > । • 11 ' ' I 1 1 ' 1 I ' • ' ' I 1 1 ' ' I 1 1 ' I ' TT ' ' 1 1 1 ■' । ’1 ■ ■ i n-p m/z 172.20 40.69% nlz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #35121:2H-Pyran-5-carboxylic acid, 2-oxo- $$ .alpha.-Pyro... 39 112 140

50001 1 ' i ' ■ 1 ' i 1 ' i ■ ’ ■ ■ i ■ ' • ■ i ■ 16.20 16.40 16.60 16.80 66 84 m/z 122.10 23.70% 49 94 0U^ ‘dd - ' i ’ 1 '' 1 1 TT7‘ 1 ' i'''11 1111'111'1 123 ■ ■ i ■ ■ ’1111 ■' i ■ ■ ■1 r A nz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #35199:1,3,5,7-Tetraazatricyclo[3.3.1.1(3,7)]decane (CAS)... 42 16.20 16.40 16.60 16.80 5000 m/z 138.10 23.54% 140 fl 49 84 — 112 35 li 98 ,l. 0- ' ■ i'' ‘11 i ■1 ■ ■ i1 ‘ •11'11 'i1 ■ i1 ''11 TIT r m/z-> 30 40 50 60 80 90 100 110 120 130 140 150 160 170 70 Abundance #35334:1,3-Cyclopentanedione, 2-acetyl- (CAS) $$ 2-ACETYL... 140 16.20 16.40 16.60 16.80 55 125 m/z44.00 21.13%

5000 MW NA 69 84 97 42 0 —PPTPP I'1 | I | !I | | T‘I" —PPp -P -mmm mtz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 16.20 16.40 16.60 16.80

01136.D HP022102.M Tue Feb 26 08:29:56 2002 Page 11 NYC-WTC_000003458

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NYC-WTC_000003458Source: NYC Law Department, mirrored locally

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