GCMS analysis results, Feb 27 2002

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Laboratory report showing GC/MS analysis results for sample AE01136 testing unknown compounds and specific analytes on February 27, 2002.

NYC-WTC_000003444–000003462

Folder label: “GCMS X 1/20/02 A 2/25/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\5973N\02FEB25\01136.D Vial: 3 Acq On : 25 Feb 2002 12:53 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ************************************************** ** ** ** * *** ** ***** * * Peak Number 8 Uracil, 5-ethyl- $$ 2,4(1H,... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T.

13.38 0.09 ug/L 55873 Naphthalene-d8 13.20

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Uracil, 5-ethyl- $$ 2,4(1H,3H)-P... 140 C6H8N2O2 004212-49-1 23 2 2,5-Diamino-6-methyl-4-pyrimidinol 140 C5H8N4O 000000-00-0 9 3 3-NITRO-4-HYDROXYPYRIDIN 140 C5H4N2O3 000000-00-0 9 4 4(1H)-Pyrimidinone, 2-amino-6-(m... 140 C5H8N40 054004-20-5 9 Abundance Scan 886 (13.376 min): 01136.D (-) m/z 140.00 100.00% 140

5000 59 93 43 70 81 121 13.00 13.20 13.40 13.60 13.80 ob ...... 149 ■ । ■ । । । । , j । । । । । > < -- TIT m/ z 59.10 27.91% n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35153: Uracil, 5-ethyl- $$ 2,4(1 H,3H)-Pyrimidinedione, 5-... 140 125 82 5000 Tii TI }ir 13.00 13.20 13.40 13.60 13.80 54 m/z93.10 24.86% 68 96 0b • । 1. । 111 ■ r< ■ ■ ■ । ■ । —Tt ■ । ■' ■11 ■11' i111' । ■1 ■1111 ■ ■ । m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35088: 2,5-Diamino-6-methyl-4-pyrimidinol 140 "IT IT 13.00 13.20 13.40 13.60 13.80 5000 m/z 70.00 19.68%

42 70 I 54 95 111 123 i 0b ■ ■ । ' ■ ■ ' । • I ■ ■ i ' 1 1 1 । ‘ - ■ ' i ' ' ■ ' i ' ''■ 1 i ' 1 ■ ' i 1 ' ' ' I ' 1 I ' ' 1 ' ' 1 i n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35073: 3-NITRO-4-HYDROXYPYRIDIN ■ i 1 ■ 1 ■ I ■ ’ 1 1 j ' 140 13.00 13.20 13.40 13.60 13.80 94 m/z 94.00 17.80% 39 5000 67 30 53 80 124

m/z-> 0b 20 +30 ।'1 ■ ■ ।11 ■ ■ । ■ 40 50 60 --HP 1i I 11 I I I . . 1 . I I 70 80 90 100 110 120 130 140 ‘II 1 — ,I 13.00 13.20 13.40 13.60 13.80

01136.D HP022102.M Tue Feb 26 08:29:56 2002 Page 10 NYC-WTC_000003457

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NYC-WTC_000003457Source: NYC Law Department, mirrored locally

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