DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004494–000004704

Folder label: “GCMS X 1/30/02 A 2/26/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB26\02091.D Vial: 8 Acq On : 26 Feb 2002 8:34 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 6, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 2-Methoxy-3-hydrazinyl-pyra... Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T.

13.38 0.05 ug/L 40375 Naphthalene-d8 13.20 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Methoxy-3-hydrazinyl-pyrazine 140 C5H8N40 000000-00-0 40 2 Pyrimidinetetramine- $$ Pyrimidi... 140 C4H8N6 001004-74-6 40 3 Uracil, 5-ethyl- $$ 2,4(1H,3H)-P... 140 C6H8N202 004212-49-1 39 4 2,5-Diamino-6-methyl-4-pyrimidinol 140 C5H8N40 000000-00-0 9 Abundance Scan 886 (13.376 min): 02091 .D (-) m/z 140.00 100.00% 140

5000

70 TT i r 1 i 1 ' ■ ' i ■ 13.00 13.20 13.40 13.60 13.80 Of .......... I. 80 84 ■ i 1 ' ■ i r■ 94 108 • 1 । i । ' 1 । । ‘ ■ i ■ ■ ■ ■ । ■ —1401 111 m/z70.00 15.05% m/z—> 30 40 50 60 70 90 100 110 120 130 Abundance #35089:2-Methoxy-3-hydrazinyl-pyrazine 140

5000 42 1 i 1 ' 1 ■ । i ■ ■ ■ - i ■

13.00 13.20 13,40 13.60 13.80 54 68 m/z 94.00 11.17% 80 95 108 121 OPP ill II I I ' ' i 1 ■ ■ i ■ ■ "T miz-> 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35040: Pyrimidinetetramine- $$ Pyrimidine, 2,4,5,6-tetraa... 140 ----------------------- 13.00 13.20 13.40 13.60 13.80 5000 m/z 96.00 11.03% 44 71 123 86 96 112 ob.. H..... TT | I I I I | T V I'l | I I I I | I1! I 1I m/z-> 30I 40 50 60 80 70 90 100 110 120 130 140 Abundance #35153: Uracil, 5-ethyl- $$ 2,4(1 H,3H)-Pyrimidinedione, 5-... > । ■ ■ > • । ■ to 13.00 13.20 13.40 13.60 13.80 125 m/z 141.10 10.22% 82 5000

54 68 96 | 111 — ob । I 1 1 I'1 I'1 1 1 1 i'1 1 1 1 I 1 1 - TII ' I 1 ' 11 I ' ' r r i 1 ‘ ' i ' m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 13.00 13.20 13.40 13.60 13.80

02091.D HP022102.M Wed Feb 27 08:35:34 2002 Page 11

NYC-WTC_000004699

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NYC-WTC_000004699Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004935

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

3 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999