GCMS analysis results for sample AE00833, Feb 2002

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Laboratory report showing GCMS analysis of sample AE00833 including surrogate recovery and unknown compounds.

NYC-WTC_000052069–000052087

Folder label: “GCMS X 1/11/02 A 1/31/02”

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NYC 9/11 Public Portal Document

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Data File : C: \MSDCHEM\1\5973N\02JAN31\00833.D Vial: 1 Acq On : 31 Jan 2002 2:42 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 Pyrimidinetetramine- $$ Pyr... Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T.

13.37 0.05 ug/L 35408 Naphthalene-d8 13.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pyrimidinetetramine- $$ Pyrimidi... 140 C4H8N6 001004-74-6 64 2 Uracil, 5-ethyl- $$ 2,4(1H,3H)-P... 140 C6H8N202 004212-49-1 59 3 4(1H)-Pyrimidinone, 6-amino-2,3-... 140 C5H8N4O 111291-90-8 50 4 2-Methoxy-3-hydrazinyl-pyrazine 140 C5H8N4O 000000-00-0 38 Abundance Scan 876 (13.375 min): 00833. D (-) m/z 140.10 100.00% 140

5000

< । - j ■ < ■ ■ । । * i • । । • 13.00 13.20 13.40 13.60 13.80 0b ,40.......... I 54 I. । . I94I , ...................-1 70......... I i 86 I. . । . I , | m/z 94.10 12.72% m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35040: Pyrimidinetetramine- $$ Pyrimidine, 2,4,5,6-tetraa... 1-0

5000 -mm— 13.00 13.20 13.40 13.60 13.80 44 71 123 m/z 96.10 11.85%

n/z-> 301 ob.....H............ 40 50 60 4 70 86 96 112 1 1 | 1 - b | ! ' I'l | ! I ! ! | I1! ! I | J, I ! | I ' 80 90 100 110 120 130 ! | 140 ""1

Abundance #35153: Uracil, 5-ethyl- $$ 2,4(1 H,3H)-Pyrimidinedione, 5-... 140 125 ■ । < ■ ■ * । ■ T-i-i-r-r-r-T-iT 82 13 00 13.20 13.40 13.60 13.80 5000 m/z 141.10 11.42%

54 68 96 0b 1 ' I ' ' ' ' I ' ' ' ' I ' ' ' 1 I ' ' ' 1 I 1 i ' ■ | । । 111 . fl । । + +L TtT n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35083:4(1H)-Pyrimidinone, 6-amino-2,3-dihydro-2-imino-1-... 'I 1 ’ 1 1 1 1 1 ■ 'I 1 ' I ' 140 13.00 13.20 13.40 13.60 13.80 43 100 m/z 70.00 9.51% 57

5000 1 68 83 111

- 0b ‘ I ■ ■ i 'I 1 1 1 1 .......... TUT’Ir ‘ ' 90 ' 100 ‘IT ■' r1^11 ' /z-> 30 40 50 60 70 80 110 120 130 140 13.00 13.20 13.40 13.60 13.80

00833 .D SCAN508.M Fri Feb 01 09:18:59 2002 Page 10

NYC-WTC_000052082

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NYC-WTC_000052082Source: NYC Law Department, mirrored locally

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