GCMS analysis results for sample AE01637, March 2002

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GCMS laboratory results for sample AE01637 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.

NYC-WTC_000010106–000010125

Folder label: “GCMS X 1/23/02 A 2/21/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB21\01637.D Vial: 6 Acq On : 21 Feb 2002 7:22 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 Pyrimidinetetramine- $$ Pyr... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T.

13.38 0.08 ug/L 54126 Naphthalene-d8 13.20

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Pyrimidinetetramine- $$ Pyrimidi... 140 C4H8N6 001004-74-6 38 2 2,5-Cyclohexadiene-l,4-dione, 2,... 140 C6H404 000615-94-1 9 3 4H-Pyran-4-one, 2-ethyl-3-hydrox... 140 C7H803 004940-11-8 9 4 2,5-Cyclohexadiene-l,4-dione, 2,... 140 C6H404 000615-94-1 9 Abundance Scan 886 (13.376 min): 01637.D (-) m/z 140.00 100.00% 140

5000

36 54 66 84 | 13.00 13.20 13.40 13.60 13.80 o! • । 44 • i ■ ■ • ■ । ■1 ■ > i *1 • > i * • * * p ...................... 134 * । * 1 * > p H * । 1 < ' 11'‘11 111 111'111 TTI m/z 96.00 15.69% miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35040: Pyrimidinetetramine- $$ Pyrimidine, 2,4,5,6-tetraa... VO

5000 ■ i ■ i ■ ■ ■ ■ i ■ 13.00 13.20 13.40 13.60 13.80 44 71 123 m/z 141.00 13.84% ,I 86 96 112

m/z-> 01 -r-p-n-r-p-r 20 30 —PPPPP 40 50 60 70 80 ----- 90 100 110 120 130 140 I—n-p Abundance #35122:2,5-Cyclohexadiene-1,4-dione, 2,5-dihydroxy- $$ p-... VO

13.00 13.20 13.40 13.60 13.80 5000 42 m/z 66.00 13.32% 71 53 84 | 94 112 0 ■ i ■' ■11 ■ • ■ ■ i ■ ‘'i ‘ ‘ i • 1 m IP i ■1•1111111 ■ ‘ ‘ i •1 iz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35347:4H-Pyran-4-one, 2-ethyl-3-hydroxy- (CAS) $$ Ethyl... vo 13.00 13.20 13,40 13.60 13.80 m/z 94.00 13.29% 5000 97 71 125 27 111 ................................... ............. 0 ■ ।■ ' TTTTI’ —PPP • p p ‘ p •••!■• TTIem 1 T’i miz-> 20 30 40 50 60> 70 80 90 100 110 120 130 140 13.00 13,20 13.40 13.60 13.80

01637.D HP022102.M Mon Feb 25 10:55:44 2002 Page 11

NYC-WTC_000010120

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GCMS analysis report for sample AE01636, March 2002 · Box DEP Box 14

NYC-WTC_000010086

GCMS laboratory results for sample AE01636 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.

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