GCMS analysis results for sample AE01637, March 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\5973N\02FEB21\01637.D Vial: 6 Acq On : 21 Feb 2002 7:22 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 2,5-DIMETHYLCYCLOHEXANE- 1,4... Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T.

16.55 0.03 ug/L 24187 Acenaphthene-dl0 18.33

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2,5-DIMETHYLCYCLOHEXANE-1,4-DION... 140 C8H12O2 000583-81-3 9 2 4H-Pyran-4-one, 2-ethyl-3-hydrox. .. 140 C7H803 004940-11-8 7 3 Methylphloroglucinol 140 C7H803 000000-00-0 5 4 2,5-Cyclohexadiene-1,4-dione, 2,... 140 C6H404 000615-94-1 4 Abundance Scan 1167 (16.548 min): 01637.D (-) m/z 140.10 100.00% 140

5000 172 43 71 122 56 89 16.20 16.40 16.60 16.80 0T 11■i'1111rr —mmpoem • ■ | • I ‘ ' I ' ' ' ‘ I -n-r-p m/z 172.20 37.12% nz—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #35634:2,5-DIMETHYLCYCLOHEXANE-1,4-DIONE $$ 1,4-Cyclohexa... 42 140

70 125 5000 55 ■ ' i ■ ■ ■ ■ i ■ ■ ‘ ■ t • ■ • ■ i ■ ■ ‘ ■ i • 16.20 16.40 16.60 16.80 m/z 43.10 29.56%

0 i‘ ' * i -n-p-r • i * ■ ■ • i ■ ■ ‘11 ■ • ■ ■ i1 ■ ■ ■ i ■ • ■ ■ i ■ ‘ —p iz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #35346:4H-Pyran-4-one, 2-ethyl-3-hydroxy- (CAS) $$ Ethyl ... 140 IT 1 ' i ■ • ■ • i ■ ■ 1 1 i ' ■ ■ ■ i ■ 16.20 16.40 16.60 16.80 5000 97 m/z 71.10 28.13% 71 125 53 84 111 0 i ■ “ ■ i ■ ■ " i ■ — Tpt — I1Asut 1 11 ■ ■ i' ■111 ■ ■'' i ■ ■ “ i * miz-> Abundance 30 40 50 60 70 80 90 1(X) 110 120 130 140 150 160 170 #35391: Methylphloroglucinol .. .....11......... 1-0 16.20 16.40 16.60 16.80 m/z 138.10 27.88%

5000 111 123 66 85 94 - Op 11111111 p । • • i •»• • i > TT-p- l < • • p ‘ ; p * * > । *1 *11 ‘ ■ ■ i • ■ ■ 1 i ■ ■ ■ • i • ■ ■ 1 i ■ ■ • ■ i 1 miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 16.20 16.40 16.60 16.80

01637.D HP022102.M Mon Feb 25 10:55:45 2002 Page 12

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