GCMS analysis results for sample AE00840, Feb 4 2002

NYC 9/11 Public Portal Document

Library Search Compound Report . Data File : C:\MSDCHEM\1\5973N\02JAN31\00840.D Vial: 4 Acq On : 31 Jan 2002 5:11 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 2,5-DIMETHYLCYCLOHEXANE-1,4... Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 16.55 0.05 ug/L 35098 Acenaphthene-dl0 18.34 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2,5-DIMETHYLCYCLOHEXANE- 1,4-DION... 140 C8H12O2 000583-81-3 38 2 Pyrimidinetetramine- $$ Pyrimidi... 140 C4H8N6 001004-74-6 37 3 Cyclohexanone, dimethylhydrazone... 140 C8H16N2 010424-93-8 37 4 Benzenethiol, 4-methoxy- $$ para... 140 C7H8OS 000696-63-9 9 Abundance Scan 1154 (16.549 min): 00840. D (-) m/z 140.10 100.00% 140

5000; 71 122 172 43 56 89 — 16 20 16.40 16.60 16.80 0 ... I,,1' i 1 ,111... i ■ ■ ■ • i ■' ... 11 ■ b ’ i 1 ■ ■......... I,,l 1 ■ ■ ■ i ■ i11111 1111111'11 IL— 11 ■ ■1 ■ ।' ■ ■ ■ । ‘ 11 m/z 172.20 30.13% m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #35634: 2,5-DIMETHYLCYCLOHEXANE-1,4-DIONE $$ 1,4-Cyclohexa... 42 140

70 125 5000 55 18 T’T 16.20 16.40 16.60 16.80 m/z 138.10 26.02% OT I ' '1111 1'11 +I I 1 ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■11 ■ ■ ■ ■ ।1

m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #35040: Pyrimidinetetramine- $$ Pyrimidine, 2,4,5 6-tetraa... 140 —r 16.20 16.40 16.60 16.80 '"I r’’"’ 1 I '

5000 m/z71.10 25.91% 44 71 123 86 96 112 OTT — ■ i ■ ■ ‘।1 P r |‘r i 1*1 [ i i i i । ' ■ i ■' ' ■ i'' ' •'' i ■ ' ' ■ I 11 1' ir ’1 ■ i' lz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #35946: Cyclohexanone, dimethylhydrazone (CAS) $$ Cyclohex... 44 140 r1 r I ' 11 1 i "‘I‘ 16.20 16.40 16.60 16.80 m/z 122.10 25.61% 5000 96 125 67 84 m/z-> O-T 30 40 111 1 ■' i ■ ■ ■ ■ i1 50 60 70 -H TT MNAII.. 80 90 100 110 120 130 140 150 160 170 I.............................. (1111 ।1 11' I '11111 । 11 । ■ ' i ' ' ' ■ i ■ ' 16.20 16.40 16.60 16.80 FTT!"i I1'I 1

>0840 .D SCAN508.M Fri Feb 01 09:19:21 2002 Page 12

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