DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004494–000004704

Folder label: “GCMS X 1/30/02 A 2/26/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB26\02090 .D Vial: 7 Acq On : 26 Feb 2002 7:45 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 6, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 2,4(1H,3H)-Pyrimidinedione,... Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 16.55 0.04 ug/L 25889 Acenaphthene-dl0 18.34 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2,4(1H,3H)-Pyrimidinedione, 1,3-... 140 C6H8N202 000874-14-6 32 2 2,5-DIMETHYLCYCLOHEXANE-1,4-DION... 140 C8H12O2 000583-81-3 32 3 2,4(1H,3H)-Pyrimidinedione, 1,3-... 140 C6H8N202 000874-14-6 9 4 1,3,5,7-Tetraazatricyclo[3.3.1.1... 140 C6H12N4 000100-97-0 9 Abundance Scan 1167 (16.548 min): 02090.D (-) m/z 140.10 100.00% 140

5000

43 71 122 172 56 89 16.20 16.40 16.60 16.80

m/z—> 0^i 11 111 ।

30 40 lul . , .I.... 50 60 70 80 90 100 110 120 130 140 150 160 170 i ■ ■1 ■ i ■' ‘' i ■' ■ i' m/z 122.10 26.74% Abundance #35147: 2,4(1 H,3H)-Pyrimidinedione, 1,3-dimethyl- (CAS)$$... 42 140 55

5000 83 ________ _ ■ i ' ' 1 ■ i ■ ■ ■ ' i ' 16.20 16.40 16.60 16.80 m/z 172.20 24.54%

/z—> O-T 30 40 50 60 70 "1I'" 70 80 JL,90.... ......... 100 110 120 130 140 150 160 170 Abundance #35634: 2,5-DIMETHYLCYCLOHEXANE-1,4-DIONE $$ 1,4-Cyclohexa... 42 140 .. n 16.20 16.40 16.60 16.80 55 70 125 m/z71.10 21.22% 5000

0 ‘ 1111 ' ' i 1 ' T-p-r '111'111' ■ ■ ■ i'' ■ ■ i'1'11111' I'11 l"........... '' r ' ‘' 11'1111'1' 11 Tl/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #35146:2,4(1 H,3H)-Pyrimidinedione, 1,3-dimethyl- $$ Uraci... TI 140 16.20 16.40 16.60 16.80 m/ Z 43.10 20.77% 55 5000 83

। 96 111 m/z—> 0 30 Pi ..... 40 50 60 Ik ... III 1 > ' | I1! i ■ । ' । I1' 11 > i-> jlf ।.।. ■ > ' ( i । '' ' ' i ■ ■ ■ ' i 1 ' 1 ■ i ' ■ ■ ■ i ' 1"I 70 80 90 100 110 120 130 140 150 160 170 16.20 16.40 16.60 16.80

02090.D HP022102.M Wed Feb 27 08:35:28 2002 Page 11

NYC-WTC_000004679

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004935

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

3 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999