GCMS DFTPP calibration report, Feb 5 2002

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Chromatogram and method report for DFTPP calibration verification conducted on February 5, 2002.

NYC-WTC_000004770–000004933

Folder label: “GCMS X 2/1/02 A 2/5/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB05\00028A.D Vial: 4 Acq On 5 Feb 2002 5:27 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP020702.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 9 Pyrimidinetetramine- $$ Pyr... Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T. 16.55 0.05 ug/L 59272 Acenaphthene-dl0 18.35 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pyrimidinetetramine- $$ Pyrimidi... 140 C4H8N6 001004-74-6 43 B_ 2 4 -HYDROXY-BI CYCLO [2.2.2] OCTANONE . . . 140 C8H1202 066348-59-2 43 3 2,5-Cyclohexadiene-1,4-dione, 2,... 140 C6H404 000615-94-1 37 4 Phenol, 4-(methylthio)- (CAS) $$... 140 C7H80S 001073-72-9 25 Abundance Scan 1154 (16.549 min): 00028A.D (-) m/z 140.20 100.00% 140

5000 172 71 122 43 56 — 89 16.20 16.40 16.60 16.80

m/z-> 01- 40 50 ■ ।1 ■ ■ 11 ■ 60 70 —2.4 80 90 98 1111 ■■1111'111 — 1’’1/1-111 i 100 110 120 130 140 150 160 170 180 i ■ ■ 11 ■ m/z 172.20 32.91% Abundance #35040: Pyrimidinetetramine- $$ Pyrimidine, 2,4,5,6-tetraa... 140

5000 1 ■ i ■ ■ ■ ' i ■ 16.20 16.40 16.60 16.80 44 71 123 m/ z 138.10 26.38% 86 96 112 0- ■ ■ i1 " " i " ।11111'h " " J1'111 1 i1 '1 * i i 1 ' ■ ' i ' n/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #35653: 4-HYDROXY-BICYCLO[2.2.2]OCTANONE $$ Bicyclo[2.2.2]... 83 140 55 70 97 112 16.20 16.40 16.60 16.80 5000 m/z 122.10 25.72%

125 0—PPPPp—T ■' i' ' ...Il 1 ■ i'1 ■ ■ i' ‘ ----- m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance i#35122:2,5-Cyclohexadiene-1,4-dione, 2,5-dihydroxy- $$ p-... 140 16.20 16.40 16.60 16.80 m/z 71.10 24.15%

5000 42 71 53 84 ,............... .................................. 94 112

m/z-> 0 T’1- 40 1 ■ i ■' 50 ..60 I,70....80I.90 100 110 120 130 140 150 160 170 180 I.. ■"...... I' 16.20 16.40 16.60 16.80

00028A.D HP020702.M Thu Feb 21 15:48:54 2002 Page 11

NYC-WTC_000004854

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