GCMS DFTPP calibration report, Feb 5 2002

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Chromatogram and method report for DFTPP calibration verification conducted on February 5, 2002.

NYC-WTC_000004770–000004933

Folder label: “GCMS X 2/1/02 A 2/5/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB05\00028A.D Vial: 4 ’ Acq On 5 Feb 2002 5:27 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\HP020702.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ***************************** * * * * ************************************ Peak Number 10 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.17 ug/L 216074 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 72 2 3-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 057102-93-9 64 3 Anthracene, 9-methyl- 192 C15H12 000779-02-2 59 4 9H-Fluorene, 9-ethylidene- (CAS) 192 C15H12 007151-64-6 59 Abundance Scan 1656 (22.280 min): 00028A.D (-) m/z 192.10 100.00% 1'12

5000

42 52 70 0 । i । । I । | 111 n i । । I H [ । । I I 82 T 118 -------mH146 160 ||Tp ... a.. / 22.00 22.20 22.40 22.60 m/z 193.10 14.77% mlz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102588:4-METHOXY-.BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192

5000 108 .... A..... 22.00 22.20 22.40 22.60 146 175 m/z 191.10 14.51%

miz-> 0 " i “ '' i'' " I " " i " " I'' " i " " I' ' 40 50 i " " I' " 11 " '' I " 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 11' " ' i " " i' Naanuil u Abundance #103424: 3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS 192 J TUl 22.00 22.20 22.40 22.60 A 5000 m/ Z 96.10 13.73%

96 164 ........ .. ............................ |......................... .................. L I | I 11 | | | 1 1 . J Lt 0 1111 niz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103921: Anthracene, 9-methyl- 192 22.00 22.20 22.40 22.60 m/z 146.10 13.44% 5000

n/z-> 0 . ... il. < I i | I » . . | I . . t ! * « 1 . | , 96 | 176 i'''' i ■ ‘ " r " ' i 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 152 165 > 11... I .'i'1 > I.. 111.. .'I u .... A - ' ' I 1 1 ‘ I 1 ' * ' I ' 22.00 22.20 22.40 22.60

00028A.D HP020702.M Thu Feb 21 15:48:54 2002 Page 12

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