GCMS DFTPP calibration report, Feb 5 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB05\00028A.D Vial: 4 Acq On 5 Feb 2002 5:27 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP020702 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 Tetradecane (CAS) $$ n-Tetr... Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 22.44 0.04 ug/L 49358 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tetradecane (CAS) $$ n-Tetradeca... 198 C14H30 000629-59-4 35 2 2-Octyldodecan-l-ol 298 C2OH420 000000-00-0 35 3 Dodecane (CAS) $$ n-Dodecane $$ ... 170 C12H26 000112-40-3 27 4 Pentadecane (CAS) $$ n-Pentadeca... 212 C15H32 000629-62-9 27 Abundance Scan 1670 (22.440 min): 00028A.D (-) m/z 57.10 100.00% 43 57 91 71 5000 105 ..... ...N.... 22.20 22.40 22.60 22.80 0 I''1' I'''' I IT ■' I ” ' 1 ] 1 ' 1 1 I 1 1 " I 1 1 1 1 I " ' 1 I 1 1 1 1 I 1 1 1 ' f 1 • I 1 I ' ' ' ■ I ' ' ' ■ I 1 1 ‘ 1 I ' ' m/z 43.10 94.17% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #113292: Tetradecane (CAS) $$ n-Tetradecane $$ Isotetradecane 43 57

5000 71 . Aln/.s 22.20 22.40 22.60 22.80 27 85 m/z 55.10 76.82% 154 99 113 127 198 0 I'11' I' 11'1'] 11 I I | I'l I I m‘ | ■ ■ ■ I | ■ I I | I I II | I > I T | I I I I | I I I I | I I I I | I 1 I

miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #248021: 2-Octyldodecan-1 -ol 57 43 T-r-p—r-r-i-p-T ■ ■ i 1 ■

71 22.20 22.40 22.60 22.80 5000 m/ Z 91.00 75.38% 85

nz—s 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #74387: Dodecane (CAS) $$ n-Dodecane $$ Ba 51 -090453 $$ Ad... A / Ajmii * 1 I ■ ' 1 ■ I ■ ' 1 1 । 43 57 22.20 22.40 22.60 22.80 m/z 41.10 60.83%

5000 71 27 85

n/z—> m 0 'l" "I ""I11111" i 113 127 140 99 170 i11" i ■r "11" " i" " i" " I" " r "' i" " i 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80

00028A.D HP020702.M Thu Feb 21 15:48:54 2002 Page 13

NYC-WTC_000004856