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GCMS analysis results for sample AE00466, Jan 18 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE00466 conducted on January 18, 2002.

NYC-WTC_000051263–000051282

Folder label: “GCMS X 1/8/02 A 1/10/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN10\00473.D Vial: 8 Acq On 10 Jan 2002 8:36 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 Pentadecane, 2,6,10,14-tetr... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 21.41 1.86 ug/L 1100900 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pentadecane, 2,6,10,14-tetramethyl- 268 C19H40 001921-70-6 91 2 Pentadecane, 2,6,10,14-tetramethyl- 268 C19H40 001921-70-6 91 3 Tetracosane, 2,6,10,15,19,23-hex... 422 C30H62 000111-01-3 91 4 Pentadecane, 2,6,10,14-tetrameth... 268 C19H40 001921-70-6 90 Abundance Scan 1580 (21.412 min): 00473.D () m/z 57.10 100.00% 57

5000 85 113 , 1 1 134 155 183201 232 21.00 21.20 21.40 21.60 21.80 39 0 T T TTTTTTTmPu m/z 71.10 77.05% " 111 z-> 40 60 80 100120140160180 200220240260280300320340 360380 400420 Abundance #211493: Pentadecane, 2,6,10,14-tetramethyl- 57

5000 i ■ ■ ■ ■ i ' ■ ' ' i ' 1 ' ■ i 85 21.00 21.20 21.40 21.60 21.80 113 m/z 43.10 46.02% । 183

J—_ O-po 1155....... 238 ................................ i > । r. । > 111 r. ।।. 111,.. 111111111 ip11111111111111 , । । 1111111111111111111111111111। ।। । i n 11 n । Tl/Z--> 40 60 80 100120140160180 200220 240260280300320340360380400420 Abundance #211490: Pentadecane. 2,6,10.14-tetramethyl- 7 i 1 1 1 1 1 1 21.00 21.20 21.40 21.60 21.80 5000 m/z 85.10 33.58% 85 113 183 0 1" r " '' 44 155 J 238 268 ' i'" ‘ i" " ii1"' i" " i ‘"11'"' i'1 ■' i ’"' i" " i"111"r' i111 r i" " i" " i'" /z-> 40 60 80 100120140160180200220 240260280300320340360380 400420 Abundance #343936: Tetracosane, 2,6,10,15,19,23-hexamethyl- (CAS) $$... F7 TT | I 21.00 21.20 21.40 21.60 21.80 m/z 41.10 21.73% 5000 85 113 183 I | J41 il .1 i ......... .............................. 395 422 0 "111" 1’1TTE’EUTTTUOTTII 1' i11111" " i" " i" " i" " r1111 i" " r "' i" " i "i" " i" "r " i 1 ■ 1 ' i ■ n/z-> 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380 400 420 2100 21.20 21.40 21.60 21.80

)0473 .D SCAN508 .M Fri Jan 11- 10:09:09 2002 Page 5

NYC-WTC_000051271

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NYC-WTC_000051271Source: NYC Law Department, mirrored locally

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