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GCMS analysis results for sample AE00466, Jan 18 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE00466 conducted on January 18, 2002.

NYC-WTC_000051263–000051282

Folder label: “GCMS X 1/8/02 A 1/10/02

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NYC 9/11 Public Portal Document

Library Search compound Report Data File : C:\MSDCHEM\1\5973N\02JAN10\00473.D Vial: 8 Acq On 10 Jan 2002 8:36 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 Pentadecane, 2,6,10-trimethyl- Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 20.61 0.62 ug/L 365905 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pentadecane, 2,6,10-trimethyl- 254 C18H38 003892-00-0 90 2 Heptacosane 380 C27H56 000593-49-7 80 3 Tridecane, 5-propyl- 226 C16H34 055045-11-9 64 4 Nonadecane (CAS) $$ n-Nonadecane 268 C19H40 000629-92-5 64 Abundance Scan 1510 (20.613 min): 00473. D (-) m/z 57.10 100.00% 57

5000 85

/z—> On 4J4441112,20 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 I " ' 'T 20.20 20.40 20.60 20.80 21.00 m/z71.10 50.86% Abundance #193195: Pentadecane, 2,6,10-trimethyl- 57

5000 20 20 20.40 20.60 20.80 21.00 85 m/z 43.10 36.73% 27 I 113 . m/z-> oU. —+4,7141 , 183 T’O’IUT 226 254 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 I''1' I' " ' I ' " ' I' ’1' I

Abundance #320678: Heptacosane 57

20'20 20.40 20.60 20.80 21.00 5000 m/ z 85.10 28.45% 85

O-mm i J 113,141 169 TTmuDT380 ’T I" " I m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #154935: Tridecane, 5-propyl- 57 20 20 20.40 20.60 20.80 21.00 m/z 41.10 17.93% 5000 85 VMwu 112 rWw~ 0- ,1)141.....183 M 1111111111111 226 1111 r " ' i " ' । ‘ । "I । ‘ ‘ ।.... p . 1111 ri i •'' ■ 11" ■ i' "' i n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 20.20 20.'40 2o'6Q 20.'80 21.00

)0473.D SCAN508.M Fri Jan 11- 10:09:09 2002 Page 4

NYC-WTC_000051270

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NYC-WTC_000051270Source: NYC Law Department, mirrored locally

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