GCMS instrument data file SCAN508, Jan 31 2002

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Library Search Compound Report

, Data File : C:\MSDCHEM\1\5973N\02JAN31\00845.D Vial: 6 Acq On : 31 Jan 2002 6:51 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************** *** * * ****** Peak Number 11 Pentadecane Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

18.43 0.21 ug/L 166609 Acenaphthene-dl0 18.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pentadecane 212 C15H32 000629-62-9 95 2 Pentadecane (CAS) $$ n-Pentadecane 212 C15H32 000629-62-9 95 3 pentadecane 212 C15H32 000629-62-9 94 4 Pentadecane 212 C15H32 000629-62-9 94 Abundance Scan 1319 (18.433 min): 00845.D (-) m/ z 57.10 100.00% 57 43 71 85 5000 A 0 w1 । । ? 113 127 141 212 18.00 18.20 18.40 18.60 18.80

m/z-> 0 H rr ri n I | MI I I I I | P. . . | . I I1' | I III |'l I I I | II I I | (I ■ I | I I । I | > ' l | ' ■ ' ■ | । | l । 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 200 210 | ‘ m/z 71.10 72.90% Abundance #134012: Pentadecane 57

71 5000 85 ----APPPPP 18.00 18.20 18.40 18.60 18.80 m/z 4 3.10 68.24%

m/z-> 0 + H, 99 113 127 141 155 I"1 ■ i1 ■1 ■ i" " I'" " i' i" ”i' 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 169 I''111 212 TTTT

Abundance #134014: Pentadecane (CAS) $$ n-Pentadecane 57 43

18.00 18.20 18.40 18.60 18.80 71 m/z85.10 53.66% 5000 85

99 —TTTTTTTTTTT '11' I " "I ""I"168 113 127 141 r " ' i" " 1111 I' mim 1111' 11' 212 0 "I 11' " ' I' H1 i"n ।11"i1 m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #134048: pentadecane 57 18.00 18.20 18.40 18.60 18.80 m/ Z 41.10 30 84% 71 | 5000 85

m/z-> OTTTT Tp 99 113 127 141 155 169 1 "| TTTT > < । h । > rr i |'i 11 11 r l‘i 11 nm 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 212 TTTT AMAudVNna— 18.00 18.20 18.40 18.60 18.80

90845.D SCAN508.M Fri Feb 01 09:19:36 2002 Page 13

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