GCMS analysis results for sample AE00466, Jan 18 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN10\00473.D Vial: 8 Acq On 10 Jan 2002 8:36 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 Pentadecane Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

23.95 0.50 ug/L 295688 Phenanthrene -dl0 22.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Pentadecane 212 C15H32 000629-62-9 95 2 Pentadecane $$ n-Pentadecane $$ ... 212 C15H32 000629-62-9 95 3 Pentadecane (CAS) $$ n-Pentadecane 212 C15H32 000629-62-9 89 4 Pentadecane (CAS) $$ n-Pentadeca... 212 C15H32 000629-62-9 81 Abundance Scan 1802 (23.947 min): 00473. D (-) m/z 57.10 100.00%

5000 43 57 71

85 A J । । 99 111193 23.60 23.80 24.00 24.20 ' . . , A .17 136, 153 168 181 .204.218 237 249 266278 . 01 '11... r > । I-Tl । IU i1 । TI । 11B । In" 1TTTNb । "f I I i । । I i r TT ri “ | i ( । ■ [ < ■ । I । iii । |^i m/z 71.10 68.96% n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #134012: Pentadecane 57

71 5000 1 । I 1 1 1 1 1 1 85 23.60 23.80 24.00 24.20 m/ z 43.10 67.05%

0- । । IP P 1 H T. 113 127 141 155 .......... . .............. .. 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #134011: Pentadecane $$ n-Pentadecane $$ CH3(CH2)13CH3 57 43 ndnn/B——T—m—n.t 71 23.60 23.80 24.00 24.20 5000 m/z 85.10 47.29%

_A 85

99 113 127 141 155 169 212 O-TT JTInT 1 i ' ■ ■ ■ i ■ ■ ■ ■ i ■ '■ ' ' f1 ' ■ '■ i ■ ■ ' ■ i ' ' ' ■ i ■ ' 1 ' i ' 1 ' 1 i ' ' 1 • i ' ' ' ' i ' '

/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #134014: Pentadecane (CAS) $$ n-Pentadecane 43 57 23.60 23.80 24.00 24.20 m/ z 41.10 26.84% 71 5000 85

99

m/z~> 0 111 ' 40 J60TTr — 80 dl 113 127 141 168 212 i ■ ■ ■ ' i ■ ■ ' ■ i ' ' ■ ' i 1 ■ ■ ■ i • ' ■ ■ i ■ ■ ' ■ i ■ 100 120 140 160180 200 220 240 260 280 1 1 1 1 ' 1 1 1 1 1 23.60 23.80 24.00 24.20 T.T

00473.D SCAN508.M Fri Jan 11 10:09:10 2002 Page 10

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