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GCMS analysis results for sample AE00466, Jan 18 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE00466 conducted on January 18, 2002.

NYC-WTC_000051263–000051282

Folder label: “GCMS X 1/8/02 A 1/10/02

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NYC 9/11 Public Portal Document

Llbrary Search compound Report Data File : C:\MSDCHEM\1\5973N\02JAN10\00473.D Vial: 8 Acq On 10 Jan 2002 8:36 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 Heptadecane $$ n-Heptadecan... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 23.86 1.39 ug/L 823301 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heptadecane $$ n-Heptadecane $$ ... 240 C17H36 000629-78-7 94 2 Octadecane (CAS) $$ n-Octadecane... 254 C18H38 000593-45-3 93 3 Octadecane 254 C18H38 000593-45-3 93 4 Tetradecane, 2,6,10-trimethyl- $... 240 C17H36 014905-56-7 91 Abundance Scan 1794 (23.856 min): 00473. D (-) m/z 57.10 100.00% 57 71

43 85 5000-

99 113 1TT ll, J, l i l 1127 141 155 171 183 197209221 238 253 278 23.60 23.80 24.00 24.20 01 ’703—0*1 ’------- m/z 71.10 82.10%

A n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #174546: Heptadecane $$ n-Heptadecane $$ Normal-heptadecane 57 71 85 5000 I 1,1 ' I' ' 23.60 23.80 24.00 24.20 99 m/ z 43.10 64.08%

m/z-> 0^ 40 J60—+ || 113,127 ........... 196... 240 80 100 120 140 160 180 200 220 240 260 280 - I > ■ I ‘ I 1 I I ■ I ■

Abundance #193187: Octadecane (CAS) $$ n-Octadecane $$ Octadecan

43 57 71 23.60 23.80 24'00 24.'20 85 5000 m/z 85.10 57.09%

99 113 127 141 155 254 0 1 I ll ll I I 197 211 227 -PPPP m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #193178: Octadecane i 1 1 1 1 i ' 1 57 2360 23.80 24.00 24.20 m/z41.10 23.86% 71 5000 85

99 113..

n/z-> 0 < ■ । 40 ■ I । > > 60 ,1. 1 . 1.147 141 155 169.183 197 210, 254 ..... . 80 100 120 140 160 180 200 220 240 260 280 i । i ! > r | l , I i । ii 23.60 23.80 24.00 24.20

0473.D SCAN508.M Fri Jan 11 10:09:09 2002 Page 9

NYC-WTC_000051275

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NYC-WTC_000051275Source: NYC Law Department, mirrored locally

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