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GCMS analysis results for sample AE01507, Mar 2002

Machine-extracted title · confidence 100%

Analytical results for sample AE01507 analyzed via GCMS on March 4, 2002, including surrogate recovery data.

NYC-WTC_000009946–000009965

Folder label: “GCMS X 1/23/02 A 2/21/02

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Scanned page image, NYC-WTC_000009960
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File : C:\MSDCHEM\l\5973N\02FEB21\01506 .D Vial: 3 Acq On : 21 Feb 2002 12:31 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 Heptadecane $$ n-Heptadecan... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

21.33 0.36 ug/L 265894 Phenanthrene-dl0 22.64

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heptadecane $$ n-Heptadecane $$ ... 240 C17H36 000629-78-7 91 2 Octadecane 254 C18H38 000593-45-3 91 3 Heneicosane $$ n-Heneicosane 296 C21H44 000629-94-7 90 4 Heptadecane 240 C17H36 000629-78-7 90 Abundance Scan 1591 (21.335 min): 01506.D (-) m/z 57.10 100.00% 57

43 71 5000 85

99 119 —--PR* 21.00 21.20 21.40 21.60 # J 113127 141 169 m/z 71.10 67.53% oM m Tkk rnfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #174546: Heptadecane $$ n-Heptadecane $$ Normal-heptadecane 57 71 85 5000 | i i C | i r i 1 | ■ l i i |^ ^ ■ | | 21.00 21.20 21.40 21.60 99 m/z 43.10 63.22% 113 127 141 196 240 .... |.l +ll 0- ’ I ‘ ‘ ‘ ‘ I • ' m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #193176: Octadecane 43 5 7 AAMc 71 21.00 21.20 21.40 21.60 5000 85 m/z 85.10 49.29%

99 119

oW- II I ■ ‘ I ."I,,. 1127 141., 169 183 197 210 24 nz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #245745: Heneicosane $$ n-Heneicosane 57 21.00 21.20 21.40 21.60 71 m/z 41.10 27.05% 85 5000

99 268 296 A AA . / Vw A ..4 /z—> 0^ 40 60 |—l 80 —100 113127 141 155 ■ ‘■ i ■ ■ ' ■ i ■ ■ ‘ ■ i ■ • ■ 11 ■ ■ ■11 ■ ■ ■ ‘ i ■ ■ • ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■'11 ■ 120 140 160 180 200 220 240 260 280 300 21.00 21.20 21.40 21.60

01506.D HP022102.M Mon Feb 25 10:54:45 2002 Page 11

NYC-WTC_000009960

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NYC-WTC_000009960Source: NYC Law Department, mirrored locally

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