GCMS analysis results for sample AE01507, Mar 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\5973N\02FEB21\01506 .D Vial: 3 Acq On : 21 Feb 2002 12:31 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 8 Decane, 5-methyl- Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 20.61 0.07 ug/L 47922 Phenanthrene-dl0 22.64

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Decane, 5-methyl- 156 C11H24 013151-35-4 38 2 Tetracontane, 3,5,24-trimethyl- 605 C43H88 055162-61-3 37 3 2-t-Butyl-3-(1-methylethenyl)oxa... 141 C8H15NO 000000-00-0 35 4 Eicosane 282 C20H42 000112-95-8 27 Abundance Scan 1527 (20.612 min): 01506.D (-) m/z 57.10 100.00% 57

5000 85 113 AM4 20.20 20.40 20.60 20.80 21.00 01 • • l‘ I •+*4*4I*I4********* m/z 85.00 34.33% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #56261: Decane, 5-methyl- 57

5000 i ■ ■ ■ ■ i 1 ■ ■ ■ i ■ ■ T • I ■ ■ 27 85 20.20 20.40 20.60 20.80 21.00 m/z 43.10 32.11% 4 156

,»A yy 0+ mz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #382447: Tetracontane, 3,5,24-trimethyl- 57 20.20 20.40 20.60 20.80 21.00 5000 m/z 41.10 27.42% 85

0- ■ ■ i ■ 111441..2385055 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #37162:2-t-Butyl-3-(1-methylethenyl)oxaziridine ■ » i * * 57 20.20 20.40 20.60 20.80 21.00 m/z 71.00 27.05%

5000 85

ii l 126 0 r ।I1। । '■ 11 । । । । । i । r । । । i । । । i । । । । । । । i । । । । । । । । । . । . . . , । . miz—> 50 100 150 200 250 300 350 400 450 500 550 20.20 20.40 20.60 20.80 21.00

01506.D HP022102.M Mon Feb 25 10:54:45 2002 Page 10

NYC-WTC_000009959