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GCMS analysis results for sample AE00843, Feb 4 2002

Machine-extracted title · confidence 90%

Laboratory report showing GCMS analysis of sample AE00843 including surrogate recovery and unknown compounds.

NYC-WTC_000052128–000052146

Folder label: “GCMS X 1/11/02 A 1/31/02

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Scanned page image, NYC-WTC_000052143
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN31\00843.D Vial: 5 Acq On : 31 Jan 2002 6:01 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

22.28 0.16 ug/L 150114 Phenanthrene-dl0 22.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 72 2 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 64 3 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 59 4 Pyrazine, tetraethyl- (CAS) $$ t... 192 C12H20N2 038325-19-8 53 Abundance Scan 1656 (22,280 min): 00843. D (-) m/z 192.10 100.00% 192

5000

on 96 146 160 ... J 22.00 22.20 22.40 22.60 40 70 82 J 120 0 11111 ■ ■ 11-11 ■ 111 > • 11 ■ ।11 ■ >111111111111 j 11 i"''I""i T‘ । raeri । n 1111111111 m/z 191.10 17.74% n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102588:4-METHOXY-BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192

5000 108 22.00 22.20 22.40 22.60 4 146 175 m/z 146.10 14.79%

0 r ■" i'' ■' i " " r ■ " i i'" ' i ■ ■" i I 111 " I " • i > > ■ ■ i ■ ■ ■ • i • ... . m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 u Abundance #88409: N-perdeuteriobenzylideneaniline 192 T A I ' ' ' ' I T 22.00 22.20 22.40 22.60 5000 82 m/z 96.10 13.76%

54 110 30 . 94 I 160 0 — I " '11 r"’i 111111 1 1111 111 11 r MT7 111 ■ 11 > -I I-1 <> 11 11 11 11....... .. । । । । | i ri l1 ‘‘1t /z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene 192 22.00 22.20 22.40 22.60 m/z 193.10 13.20%

5000

96 165

m/z-> 0 88 J ■' i " ■' i" '' i' ■ " i" " r '" r ■'1 r 139 152 ' i " ■ ■ r ' ■' i " ■ ■ i" " r '" i1' ■ ■ i 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 ,| 176 . ■ ■ i "1 ■ i'1 ,'11 U Tid 22.00 22.20 22.40 22.60

00843.D SCAN508.M Fri Feb 01 09:19:28 2002 Page 12

NYC-WTC_000052143

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NYC-WTC_000052143Source: NYC Law Department, mirrored locally

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