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GCMS results for sample AE00740, Jan 29 2002

Machine-extracted title · confidence 100%

GCMS analysis log for sample AE00740 showing surrogate recovery and unknown compounds detected on January 29, 2002.

NYC-WTC_000051984–000052000

Folder label: “GCMS X 1/10/02 A 1/16/02

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Scanned page image, NYC-WTC_000051998
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NYC 9/11 Public Portal Document

Library Search Compound Report ’ Data File : C:\MSDCHEM\1\5973N\02JAN16\00740.D Vial: 8 Acq On : 16 Jan 2002 8:57 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ****************************** * * * * * * * ******************************** Peak Number 9 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.14 ug/L 94635 Phenanthrene-dl0 22.65 Hit# Of 5 Tentative ID MW MolForm • CAS# Qual

1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 72 2 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 64 3 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 53 4 3-(2-Methoxy-5-methylphenyl)acry... 192 C11H1203 103986-76-1 53 Abundance Scan 1656 (22.280 min): 00740.D (-) m/z 192.10 100.00% 192

5000

96 146 160 ■ ' i ' ■ ' ■ i 1* r 70 82 /z-> 0 118 TmTTT Mil.. . i11" i'111111 ..... 1....1. 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 l 22.00 22.20 22.40 22.60 m/z 191.10 17.39% Abundance #102588: 4-METHOXY-.BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192

108 5000 22.00 22.20 22.40 22.60 146 175 m/z 96.00 15.88%

m/z-> 0 i'''' i''1' r " ' i ■' ' r ■ " i'1" r I.. . 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance u #88409: N-perdeuteriobenzylideneaniline 192

22.00 22.20 22.40 22.60 5000 82 m/z 146.10 15.64% 54 110 30 1 94 160 m/z-> 0m20r .. mlerpll ... "I" "I" '" i ■ " ' i" .... .|।।. I 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 TIT"

Abundance #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene A i ■ • ■ ■ i J 192 22.00 22.20 22.40 22.60 m/z 193.10 13.87% 5000

n/z-> 0 96 88 J 139 152 ‘I‘1"TT*1*T*TnImnmmuumemtmpmmh 155 । 176 , 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 u 22.00 22.20 22.40 22.60

30740.D SCAN508.M Thu Jan 17 08:17:59 2002 Page 11

NYC-WTC_000051998

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NYC-WTC_000051998Source: NYC Law Department, mirrored locally

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