GCMS analysis results for sample AE00830, Feb 2002

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Laboratory report showing GCMS analysis of sample AE00830 including surrogate recovery and unknown compounds.

NYC-WTC_000052047–000052068

Folder label: “GCMS X 1/11/02 A 1/31/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C : \MSDCHEM\1\5973N\02JAN31\00830.D Vial: 3 Acq On : 31 Jan 2002 12 :11 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.16 ug/L 125891 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H12O3 019169-94-9 72 2 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 59 3 6-Methoxy-2,4-dihydroxy-1,5-naph... 192 C9H8N2O3 000000-00-0 50 4 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 50 Abundance Scan 1656 (22.280 min): 00830.D (-) m/z 192.10 100.00% 192

5000

82 96 146 1 1 I ■ ■ 1 1 r1 ■ 160 22.00 22 20 22.40 22.60 42 70 | 118 0 ..... I '■■ ■ ...... . . M 1111 ■ । ■ It i ■' ■ ■ T" ■ i|.............. [Hl ■■ i. ■ ■ । i ■1111 ■ 1111111 ■ [' Ip m/z 191.10 19.28% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102588: 4-METHOXY-.BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192

108 5000 ‘ ————TCTDd/n/n/nn—k. 22.00 22.20 22.40 22.60 146 175 m/z 146.10 16.90% 0 i ■''' i ■''' i' ■'' r ■ ■ I ■' ■ ■ [ I I >' 11 IUnu Tpn m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline 192 A I ■ ' I « I TTTr 22.00 22.20 22.40 22.60 5000 82 m/z 96.10 16.67% 54 110 30 0 mPP mPH . ................................160 I 94 I........... "I1"'1' m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102277:6-Methoxy-2,4-dihydroxy-1,5-naphthyridine 10/20/——— 192 22.00 22.20 22.40 22.60 m/z 193.10 14.22% 5000 52 80 149 163 108 12 122 134 0 " i " '' i1' " i "r"'r' •' r ■ " i " 1..... 1 l1" 1 f - I' " ' i" " I TTmm17 n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

00830.D SCAN508.M Fri Feb 01 09:18:32 2002 Page 13

NYC-WTC_000052063

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NYC-WTC_000052063Source: NYC Law Department, mirrored locally

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GCMS analysis results for sample AE00840, Feb 4 2002 · Box DEP Box 28

NYC-WTC_000052108

Laboratory report showing GCMS analysis of sample AE00840 including surrogate recovery and unknown compounds.

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