GCMS DFTPP calibration report, Feb 5 2002

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Chromatogram and method report for DFTPP calibration verification conducted on February 5, 2002.

NYC-WTC_000004770–000004933

Folder label: “GCMS X 2/1/02 A 2/5/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB05\29232A.D Vial: 4 Acq On 5 Feb 2002 1:13 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 4-METHOXY-.BETA.-METHYLCINN. .. Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.18 ug/L 226030 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 64 2 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 59 3 6-Methoxy-2,4-dihydroxy-1,5-naph... 192 C9H8N2O3 000000-00-0 50 4 1,4-Dimethyl-3,5-propanobicyclo[... 192 C13H20O 000000-00-0 47 Abundance Scan 1656 (22.280 min): 29232A.D (-) m/z 192.10 100.00% 1912

5000

96 160 146 46 54 70 82 , 108 118 | 22.00 22.20 22.40 22.60 0 .. ............................ .. 1111; [. i r 1111. ■ 1 '' ’ I’"1" I.... 11... I1 m/Z 191.10 18.06% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102588:4-METHOXY-BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192

5000 108 / \ I ' ‘ 1 22.00 22.20 22.40 22.60 ... A 1" ’ I ’ I

146 175 m/z 96.00 15.57%

/z—> 0 111‘11111—311"10113E110‘TTI——III"II11T ....... . 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 k Abundance #88409: N-perdeuteriobenzylideneaniline 192 ......................................... 22.00 22.20 22.40 22.60 5000 82 m/z 146.10 14.87%

54 110 30 160 0 "■'I"......... " i " " r l 94 -H " i " 1' i " " i " " I ‘ nap...... 1 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102277: 6-Methoxy-2,4-dihydroxy-1,5-naphthyridine 192 -A 22.00 22.20 22.40 22.60 m/z 193.10 13.28%

5000 52 80 149 163 108 4 29 122 134 0 " i " ■ ■ i" " i " i" " i" 1.... 1 - 111 "I"" I" " I 1..... ■' r ‘ ‘ ■ i'' 11'' " I ' " I'1 / m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 1 60 170 180 190 200 22.00 22.20 22.40 22.60

29232A.D SCAN508.M Fri Feb 22 11:44:19 2002 Page 14

NYC-WTC_000004893

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