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GCMS DFTPP calibration report, Feb 5 2002

Machine-extracted title · confidence 95%

Chromatogram and method report for DFTPP calibration verification conducted on February 5, 2002.

NYC-WTC_000004770–000004933

Folder label: “GCMS X 2/1/02 A 2/5/02”

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Scanned page image, NYC-WTC_000004892
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB05\29232A.D Vial: 4 Acq On 5 Feb 2002 1:13 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 Pyrimidinetetramine- $$ Pyr... Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 16.55 0.05 ug/L 53458 Acenaphthene-dl0 18.34 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pyrimidinetetramine- $$ Pyrimidi... 140 C4H8N6 001004-74-6 38 2 4(1H)-Pyrimidinone, 2-amino-6-et... 155 C6H9N3O2 042956-82-1 9 3 .beta.,beta.-Difluorostyrene 140 C8H6F2 000000-00-0 9 4 .beta. ,beta.-Difluorostyrene 140 C8H6F2 000000-00-0 9 Abundance Scan 1154 (16.549 min): 29232A.D (-) m/z 140.20 100.00% 140

5000 172 122 43 56 71 16.20 16.40 16.60 16.80 '' n/z-> ol 40 50 TI‘41‘1‘11 TT 89 - , 150 Pl 60 70 80 90 100 110 120 130 140 150 160 170 TT-p L m/z 172.10 37.41% Abundance #35040: Pyrimidinetetramine- $$ Pyrimidine, 2,4,5,6-tetraa... 140

5000 16.20 16.40 16.60 16.80 44 71 123 m/z 138.10 24.96% 86 96 112 01 TI11 1111111111 111111 > ।' > I'l ।... 11 Ih " । J, ।, 11 11' ■ ■ ■ i ■ ■' ■ i ‘ m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #53874:4(1 H)-Pyrimidinone, 2-amino-6-ethoxy- 140 86 155 . .......II.......... 127 16.20 16.40 16.60 16.80 5000 m/z 122.10 24.37% 99 111 42 70

01 TITT 1 ' i 1 ' 11" 1111" 1111" i11 I, Pri i'111111'111'' 111 m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #35448: .beta.,beta.-Difluorostyrene 140 16.20 16.40 16.60 16.80 m/z 136.10 18.49% 90 5000

114

m/z-> 0 ............. . 101 11111 ■111111111'11 *1 *111111 - L. ■' i'' ■11 ■ ■ ■ ■ i ■ ■ ■111 40 50 60 70 80 90 100 110 120 130 140 150 160 170 16.20 16.40 16.60 16.80

29232A.D SCAN508.M Fri Feb 22 11:44:19 2002 Page 13

NYC-WTC_000004892

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NYC-WTC_000004892Source: NYC Law Department, mirrored locally

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

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