GCMS analysis results for sample AE00839, Feb 4 2002

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Laboratory report showing GCMS analysis of sample AE00839 including surrogate recovery and unknown compounds.

NYC-WTC_000052088–000052107

Folder label: “GCMS X 1/11/02 A 1/31/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN31\00839.D Vial: 3 Acq On : 31 Jan 2002 4:21 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 12 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.16 ug/L 142151 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 64 2 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 59 3 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 53 4 l-amino-2-methyl-4-isopropyl-thi... 192 C5H13N4PS 107264-54-0 50 Abundance Scan 1656 (22.280 min): 00839. D (-) m/z 192.10 100.00% 192

5000

96 ■ ■ i ■ • >»r ■ ■ 146 160 । /z—> 0 AO 42 . 51 ■11 • ■ ■ • | 1 ■ pp 00 82 I ।1 H , |..!. । J i!. ।. 11’. Hm 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 118 pr Aogvaskstsiyoaspann)) II— "z 22.00 22.20 22.40 22.60 96.10 19.02% Abundance #102588:4-METHOXY-.BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192

108 -.. .......... .............. .... 5000 22.00 22.20 22.40 22.60 146 175 m/z 191.10 15.99% 0 I'' ’' I 11''11 1′11 ' I ‘ 'I i " " i " " I" " r ' ■ i" " i ■ " ' r 11. ...... TI’1 n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene 192

22.00 22.20 22.40 22.60 5000 m/z 146.10 14.49%

96 165 88 al 139 152 176 0 111 ''1 ’ f " r 1 1 11" I' JrTTTTHTTTT TTT f P •»> j»।»»। < i l • ।«। < < 11. ।। • i i 111»। r11 111 11»111

n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline 192 22.00 22.20 22.40 22.60 m/z 193.10 14.25% 5000 82

54 110 30 94 160 0 -T " i" " r ' " i -H mPTT TETTTTT /z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

30839.D SCAN508.M Fri Feb 01 09:19:15 2002 Page 14

NYC-WTC_000052105

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Laboratory report showing GCMS analysis of sample AE00832 including surrogate recovery and unknown compounds.

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