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GCMS analysis results for sample AE00839, Feb 4 2002

Machine-extracted title · confidence 90%

Laboratory report showing GCMS analysis of sample AE00839 including surrogate recovery and unknown compounds.

NYC-WTC_000052088–000052107

Folder label: “GCMS X 1/11/02 A 1/31/02

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Scanned page image, NYC-WTC_000052104
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN31\00839.D Vial: 3 Acq On : 31 Jan 2002 4:21 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 Tetradecane (CAS) $$ n-Tetr... Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T.

18.43 0.13 ug/L 109893 Acenaphthene-dl0 18.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tetradecane (CAS) $$ n-Tetradeca... 198 C14H30 000629-59-4 83 2 Heptadecane 240 C17H36 000629-78-7 83 3 pentadecane 212 C15H32 000629-62-9 83 4 Heptadecane (CAS) $$ n-Heptadeca... 240 C17H36 000629-78-7 83 Abundance Scan 1319 (18.433 min): 00839.D (-) m/z 57.10 100.00% 57

43 71 5000 85 .A. .D/, A 99 18.00 18.20 18.40 18.60 18.80 0 1 1 1 1 1 TIdT m/ z 43.10 62.61% m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #113303: Tetradecane (CAS) $$ n-Tetradecane $$ Isotetradecane 43 57

5000 71 Ny YM ft, A AM I 85 18.00 18.20 18.40 18.60 18.80 m/z 71.10 62.42% 0 | ' | ' r I ■ . ' I | ' r , 99 113 127 141 154 1?8 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #174552: Heptadecane 57 43

71 18.00 18.20 18.40 18.60 18.80 5000 m/z 85.20 43.91% 85

H 99 113 1 27 141 240 0-PPTT —1 80m— T———BmOTNTTTTDOOOTTT 100 120 140 160 180 200 220 240 m/z-> 20 40 60 Abundance #134046: pentadecane i 1 1 ■ ' i T 43 57 18.00 18.20 18.40 18.60 18.80 m/z 41.10 31.65% N 5000 71

85

m/z-> 0-PP 20 27

40 — 60 . 99 113 127 212 ' i । 1 1 1,11 1 1 111 i 1'' 1 1 i 1 1 1 1 i 1 1 1 1 i 1 1 1 1 । ■ ' 1 1 i ■ • 1 1 i ' ■ 80 100 120 140 160 180 200 220 240 .A— 18.00 18.20 18.40 18.60 18.80

00839.D SCAN508.M Fri Feb 01 09:19:15 2002 Page 13

NYC-WTC_000052104

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NYC-WTC_000052104Source: NYC Law Department, mirrored locally

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