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GCMS analysis results for sample AE00839, Feb 4 2002

Machine-extracted title · confidence 90%

Laboratory report showing GCMS analysis of sample AE00839 including surrogate recovery and unknown compounds.

NYC-WTC_000052088–000052107

Folder label: “GCMS X 1/11/02 A 1/31/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN31\00839.D Vial: 3 Acq On : 31 Jan 2002 4:21 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 Hexadecane Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

15.19 0.09 ug/L 68565 Naphthalene-d8 13.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexadecane 226 C16H34 000544-76-3 83 2 Tetradecane (CAS) $$ n-Tetradeca... 198 C14H30 000629-59-4 83 3 Tetradecane (CAS) $$ n-Tetradeca... 198 C14H30 000629-59-4 83 4 Tridecane (CAS) $$ n-Tridecane $... 184 C13H28 000629-50-5 83 Abundance Scan 1035 (15.190 min): 00839.D (-) m/z 57.10 100.00% 57

43 71 5000 85 401117 „/ , ,44 nA, 99 14.80 15.00 15.20 15.40 15.60 Ml —H il ................................................................................. m/ z 43.10 66.09% m/z-> 0-TTT Abundance 20 20 60 80 100 120 140 #154905: Hexadecane 160 180 200 220 57 43

71 1 nP MP two A7A, 5000 14.80 15.00 15.20 15.40 15.60 85 m/z 71.10 57.74%

0- I 1 1 rp .. ml PT 99 113 127 ■ i ' 1 ' ' i ' ' • ' i ■ ' ■ ■ i ■ 1 ‘ ' I 226 1 1 n/z- > ;20 40 60 80 100 120 140 160 180 200 220 Abundance #113302: Tetradecane (CAS) $$ n-Tetradecane $$ Isotetradecane 43 57 A TI0dmdm03sI1—T I 14.80 15.00 15.20 15.40 15.60 5000 71 m/z 85.10 32.06% 85 A 27 __ | 99 113 127 198 0- i ' ' ' 1 1 1 '■ 1 I ' ' —by /z->20 40 60 80 100 120 140 160 180 200 220 \ ........................... ............. . Abundance #113303: Tetradecane (CAS) $$ n-Tetradecane $$ Isotetradecane 43 . 57 14.80 15.00 15.20 15.40 15.60 m/ z 41.10 30.78% 71 5000 85

99 113 127 141 154 198 n/z—> OM 1 rT' 20 40 MM 60 80 100 120 140 160 180 200 220 14.80 15.00 15.20 15.40 15.60

00839.D SCAN508.M Fri Feb 01 09:19:15 2002 Page 12

NYC-WTC_000052103

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NYC-WTC_000052103Source: NYC Law Department, mirrored locally

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