GCMS analysis results for sample AE00839, Feb 4 2002

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Laboratory report showing GCMS analysis of sample AE00839 including surrogate recovery and unknown compounds.

NYC-WTC_000052088–000052107

Folder label: “GCMS X 1/11/02 A 1/31/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN31\00839.D Vial: 3 Acq On : 31 Jan 2002 4:21 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 9 Dodecane (CAS) $$ n-Dodecan... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 13.41 0.41 ug/L 323201 Naphthalene-d8 13.19 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Dodecane (CAS) $$ n-Dodecane $$ ... 170 C12H26 000112-40-3 90 2 Dodecane (CAS) $$ n-Dodecane $$ ... 170 C12H26 000112-40-3 87 3 Dodecane (CAS) $$ n-Dodecane $$ ... 170 C12H26 000112-40-3 87 4 Dodecane (CAS) $$ n-Dodecane $$ ... 170 C12H26 000112-40-3 87 Abundance Scan 879 (13.409 min): 00839.D (-) m/z 57.10 100.00% 57 43

71 5000 85

98 113 127 i40 170 13.00 13.20 13.40 13.60 13.80

m/z-> O-TTTT —4 +Tmr 4TT — lank r1 i । " 1 ■' ■ M ■11 > M 11 ■ 11 pi 11 > । > 11111 ■ > 11' 11 ■ । 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 m/z43.10 70.21% Abundance #74405: Dodecane (CAS) $$ n-Dodecane $$ Ba 51-090453 $$ Ad... 4)3 57

— . 5000 71 13.00 13.20 13.40 13.60 13.80 85 m/ z 71.10 50.21% 27 — 98 112 127 170 01 ’I’’ TRTTTI PTItaup 1 ''' i ' ' 1 1 i 1 ' ' ‘ i ' 1 1 • i ■ ■ 1 ■ 1 1 ' 1 ' i m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #74393: Dodecane (CAS) $$ n-Dodecane $$ Ba 51-090453 $$ Ad... 43 57 /, '■

“f 13.00 13.20 13.40 13.60 13.80 5000 71 m/z 85.10 33.35% 85 27

rnlz-> 0 20 —

30 md , 99 113 127 170 TI—OPu——n—pu——mewn———m—nn—nnemunn—Ton] 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #74404: Dodecane (CAS) $$ n-Dodecane $$ Ba 51-090453 $$ Ad... 2 I '-T-' 1 I ' 1 । 1 | । ! I I’I’t —P4 43 57 13.00 13.20 13.40 13.60 13.80 m/z 41.10 29.30% 5000 71 1 85

m/z-> o ■ i"111" " 11 20 30 40 m 50 ■ i ‘

60 | 98 113 127 141 ■ i ■ ■ •' i ■।, 111'| 11111 i'i 1111 > i'i 1... .. ..... ........... .....

70 80 90 100 110 120 130 140 150 160 170 1/0 1111| ।, 11 —A S 13.00 13.20 13.40 13.60 13.80

00839.D SCAN508.M Fri Feb 01 09:19:14 2002 Page 11

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GCMS analysis results for sample AE00832, Feb 4 2002 · Box DEP Box 28

NYC-WTC_000052147

Laboratory report showing GCMS analysis of sample AE00832 including surrogate recovery and unknown compounds.

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