GCMS analysis results for sample AE00103, Jan 2002

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Laboratory report for sample AE00103 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.

NYC-WTC_000050384–000050396

Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN23\00103.D Vial: 5 Acq On : 23 Jan 2002 6:15 pm Operator: Sample : 508 scan Inst : Instrumen . Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L * * * ****************************************************************** Peak Number 3 Dodecane (CAS) $$ n-Dodecan... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 9.45 0.12 ug/L 43058 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Dodecane (CAS) $$ n-Dodecane $$ ... 170 C12H26 000112-40-3 64 2 Dodecane (CAS) $$ n-Dodecane $$ ... 170 C12H26 000112-40-3 64 3 Tridecane (CAS) $$ n-Tridecane $... 184 C13H28 000629-50-5 64 4 Undecane (CAS) $$ n-Undecane $$ ... 156 C11H24 001120-21-4 64 Abundance Scan 532 (9.447 min): 00103.D (-) m/z 57.10 100.00% 43 57

5000 71 85 281 ......... A..... 9.00 9.20 9.40 9.60 9.80 0-1 ■ ■ i * ■ ■ ‘ i ‘ ■ •11 • ■ ■ ■ i ■ •' ■ i ‘ • • • i1 ‘1 ‘ i ‘ ■ ■ • i ■ ■ ■11 ‘ ■1 ■ i11 ■' i * ■ m/z 43.10 92.54% z-> 20 80 100 120 140 160 180 200 220 240 260 280 Abundance #74388: Dodecane (CAS) $$ n-Dodecane $$ Ba 51-090453 $$ Ad... 43 57

5000 71 . ......... MANA(, 27 85 9.00 9.20 9.40 9.60 9.80 1 m/z 71.10 42.89% 0-' i • ■ •11 ■ • 1.1/.99.113127140170......................... /z—> :20 40 60 80 ’ 100 120 140 160 180 200 220 240 260 280 Abundance #74401: Dodecane (CAS) $$ n-Dodecane $$ Ba 51-090453 $$ Ad... 43 57 i ■ ■ ■ ' i ■ ■ 1 1 i ■ • ■ ‘ i ' ■ ■ ■ i ■ ■ • 9.00 9,20 9.40 9.60 9.80 5000 71 m/z 41.10 31.29% 85 i NAA -Hr 99 113127 170 O' i • •1 • 1" ■ il i .i । ‘18 -184/8/— j • ‘ TTO8T4 J • « J I j » I J I J 4 • < I j I * I I j l I l [4 4 111* /z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #93363: Tridecane (CAS) $$ n-Tridecane $$ Tridecane, n- । ■ ■ ■ 11 ■■■■।■1■■।■i‘11 43 57 9.00 9.20 9.40 9.60 9.80 m/z 85.10 24.54% | 5000 71 27 85

0 । i ■11 |"i ■ 1199 113 127 141 154 184...................... m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 9.00 9.20 9.40 9.60 9.80

00103.D SCAN508.M Thu Jan 24 09:57:18 2002 Page 5

NYC-WTC_000050392

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