GCMS analysis results for sample AE00832, Feb 4 2002

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Laboratory report showing GCMS analysis of sample AE00832 including surrogate recovery and unknown compounds.

NYC-WTC_000052147–000052166

Folder label: “GCMS X 1/11/02 A 1/31/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN31\00832.D Vial: 5 Acq On : 31 Jan 2002 1:52 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 Dodecane (CAS) $$ n-Dodecan... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 13.41 0.35 ug/L 273983 Naphthalene-d8 13.19 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Dodecane (CAS) $$ n-Dodecane $$ ... 170 C12H26 000112-40-3 93 2 Dodecane (CAS) $$ n-Dodecane $$ ... 170 C12H26 000112-40-3 91 3 Dodecane $$ n-Dodecane $$ Adakan... 170 C12H26 000112-40-3 91 4 Dodecane (CAS) $$ n-Dodecane $$ ... 170 C12H26 000112-40-3 90 Abundance Scan 879 (13.409 min): 00832.D (-) m/z 57.10 100.00% 57 h 43

71 5000 85 A TTTrTTr 7 1 1 ' ' ITTTrn 13.00 13.20 13.40 13.60 13.80 , 99 112 127 140 170 0 । Pr 111 rl 4 r Tmmmmmmtn m/ z 43.10 74.17% n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #74398: Dodecane (CAS) $$ n-Dodecane $$ Ba 51-090453 $$ Ad... 43 5(7

71 5000 13.00 13.'20 13.40 13.60 13.80 85 m/z 71.10 52 92% | 99 113 127 141 170 01 11111111 r 1' i111' i ■ ■1 ’ i ’ TITTITITOTTTPTWPPTIPTITTT m/z-> 20 30 40 50 60 80 90 100 110 120 130 140 150 160 170 Abundance #74407: Dodecane (CAS) $$ n-Dodecane $$ Ba 51-090453 $$ Ad...

43 57 _-4 71 13.00 13.20 13.40 13.60 13.80 5000 m/z 85.10 34.98% 85

n/z-> 13271 0 11114′1111111141115111 1 1 ■ i'1 ■' i'1 '11' ■'' i1'' ■ i ■ ■'11 " ' ‘ i' ’111111 ‘ i'1 20 30 40 50 60 7080 90 100 110 120 130 140 150 160 170 170 T’i

Abundance #74403: Dodecane $$ n-Dodecane $$ Adakane 12 $$ Ba 51-0904... -----AAA 43 57 13.00 13.20 13.40 13.60 13.80 "/Z 41.10 33.64% 71 5000 85 27 I 98 112 126 0 U1 1 11 I' 1 ' 11 1 TTTT' ’ TTTT ■ I' ■ ■' i'11' i " '11 ■11111111111111 " 111" 1 '"111111'1 ri I11111 170 ' I ' 1 ' 1 1 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 13.00 13.20 13.40 13.60 13.80

30832.D SCAN508.M Fri Feb 01 09:18:52 2002 Page 7

NYC-WTC_000052157

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GCMS analysis results for sample AE00839, Feb 4 2002 · Box DEP Box 28

NYC-WTC_000052088

Laboratory report showing GCMS analysis of sample AE00839 including surrogate recovery and unknown compounds.

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