GCMS analysis results for sample AE00832, Feb 4 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN31\00832.D Vial: 5 Acq On : 31 Jan 2002 1 :52 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 4 DIETHYLAMINE-DI Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 9.86 0.24 ug/L 129219 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

I DIETHYLAMINE-D1 74 C4H10DN 000997-11-5 64 2 PROPYLENE GLYCOL TRIMER 1 174 C9H18O3 000000-00-0 56 3 2-Propanol, 1,1‘-[(1-methyl-l,2-... 192 C9H20O4 001638-16-0 43 4 Acetic acid, ethoxy-, 1-methylet ... 146 C7H14O3 054063-13-7 40 Abundance Scan 568 (9.858 min): 00832.D (-) m/z 59.10 100.00% 59

5000

45

n/z-> 0—T 20 30 l 1 40___ 50 60 84 ' i 1 ' ‘ ' i ■ ' ' 1 i ‘ ‘ 70 73

80 90 103 103 ■ i ’ 1 ' 1 i ■ 1 1 1 i 1 1 1 ' i 1 100 110 120 130 9.60 m/z45.10 9.80 10.00 10.20 15 77% Abundance #1887: DIETHYLAMINE-D1 31 59

5000 TOR 74 9.60 9.80 10.00 10.20 45 m/ z 58.00 11.61% , I I' — 0 ‘ I ' ' 11 ' I ■ ' •1 i 1 m/z-> 20 30 40 50 (60 70 80 90 100 110 120 130 Abundance #78532: PROPYLENE GLYCOL TRIMER 1 59 ■ ' • ' i ■ ■ 1-I■' 9.60 9.80 10.00 10.20 5000’ 41 m/z42.10 10.58% 103

73 0-5 ! 1 1 1 ! | I 1 1 1 | ----- 1i■ • 87 i ■ ' 1 r i' 1 ' ' i ■ ■ 117 130 ' ■ i ■ ' ' 1 i ■ 1 n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #102318:2-Propanol, 1,1'-[(1-methyl-1,2-ethanediyl)bis(ox... 53 9.60 9.80 10.00 10.20 m/z 41.10 9.71%

5000 31 45 103 39 | 73 0l I 1 i ■ 1 ' ' i 1 '■'-'‘i i' "'h, ■' TTPpT ■ 1 i 1 • • • । ■ I > > i ■ • 117 ■' > i ' ■ ■ • i ■ ■ /z-> 20 30 40 50 60 70 80 90 100 110 120 130 9.60 9.80 10.00 10.20

00832.D SCAN508.M Fri Feb 01 09:18:52 2002 Page 6

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