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GCMS analysis results for sample AE00832, Feb 4 2002

Machine-extracted title · confidence 90%

Laboratory report showing GCMS analysis of sample AE00832 including surrogate recovery and unknown compounds.

NYC-WTC_000052147–000052166

Folder label: “GCMS X 1/11/02 A 1/31/02

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Scanned page image, NYC-WTC_000052155
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\5973N\02JAN31\00832.D Vial: 5 Acq On : 31 Jan 2002 1:52 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 2-Pentanone, 4-amino-4-meth... Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 7.15 0.21 ug/L 113473 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone, 4-amino-4-methyl- (... 115 C6H13NO 000625-04-7 83 2 2-Pentanone, 4-amino-4-methyl- $... 115 C6H13NO 000625-04-7 64 3 .alpha.-Pinene, 10-(dimethylamin... 193 C13H23N 000000-00-0 9 4 AZETIDINE-Dl 58 C3H6DN 024847-27-6 7 Abundance Scan 331 (7.153 min): 00832.D (-) m/z 58.10 100.00%

M. 53

5000 43 100 1 1 ! 1 1 T ' 1 1 TT 6.80 7.007.20 7.40 7.60 III,.,,,,, 84 I 0 11" " i11 ‘ 11 111'11 11 > 111111 nHrmTTT 11 m/ z 43.10 30.25% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #15911:2-Pentanone, 4-amino-4-methyl- (CAS) $$ DIACETONEA... 58 NowWA 5000 43 6 80 7.00 7 20 7.40 7.60 m/z 42.10 15.08% 0 ' l" 1115571111 1111 -mmP 84 100 TTImn—mn’uum———nmuOu Nwp n/z-> Abundance 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 #15910: 2-Pentanone, 4-amino-4-methyl- $$ Diacetonamine 58 W 6.80 7.00 7.20 7.40 7.60 5000 m/z 100.00 11.71%

n/z-> 30 I 42

0------ ,TTOTTUT— 84 _ TtTT 100 I —TTUTgTTTTTTTTIi :20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 MMasii Abundances #104688: .alpha.-Pinene, 10-(dimethylaminomethyl)- ‘ 17/1 f V ' ' I 1 ' ' I ' ' 58 6 80 7.00 7.20 7.40 7.60 m/ Z 9.46%

5000

30 77 91 193 oV TTmTuuntuNUTmT r i ' 1 ■ ■ i ' TI—I n/Z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 6.80 7.00 7.20 7.40 7.60

00832.D SCAN508.M Fri Feb 01 09:18:51 2002 Page 5

NYC-WTC_000052155

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NYC-WTC_000052155Source: NYC Law Department, mirrored locally

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