GCMS analysis results for sample AE00838, Feb 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN31\00831.D Vial: 4 Acq On : 31 Jan 2002 1:01 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 2-Pentanone, 4-amino-4-meth... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

6.68 3.34 ug/L 1457280 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-amino-4-methyl- $... 115 C6H13NO 000625-04-7 78 2 2-Pentanone, 4-amino-4-methyl- ( . .. 115 C6H13NO 000625-04-7 64 3 1-Propanol, 2-amino-2-methyl- (C... 89 C4H11NO 000124-68-5 50 4 Permethylspermine 286 C16H38N4 057905-96-1 40 Abundance Scan 290 (6.685 min): 00831 .D (-) m/z 58.10 100.00% 58

5000 43 f • i • । • • ■ ■ । ' । ■ ■ ■ i ' ■ 1 1 100 6.40 6.60 6.80 7.00 83 । Or Tumurr n । th l| I - Ip #4 ■ i"111" ■' i1" ■i■'1'i'11' i1'1 ■ i'1' m11' I" m/ z 43.10 29.20% m/z~> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #15910:2-Pentanone, 4-amino-4-methyl- $$ Diacetonamine $$... 58

5000 = , 44 ' I ' ' ' I ' ' 1 ' 6.40 6.60 ।6.80 7.00 42 m/ z 42.10' 17.38%

P 30 .35 | 49 _ 100 , 84 1 Of' ■ " I ■ ■ " | I 1 ■ ■ | I ' > I | 1 I > | I M IMTTTTH 1111111 in 11,.., । im , ।,.. 111. i. ।.... 1111 , 11 > 111 ■ m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #15911: 2-Pentanone, 4-amino-4-methyl- (CAS) $$ DIACETONEA... 58 ' ’ 'If >1 rill1. .1 I n I I"! -Ill 1 6.40 6.60 6.80 7.00 5000 m/z 100.10 10.74% 43 M m/z—> OfTT"TTT 49 84 100 | Multi- I [ n n | u u 11 u (111111 n 7l (ITTi | n ' > | u i, I n ■ 11 >, 11 r 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance W #5062:1-Propanol, 2-amino-2-methyl- (CAS) $$ 2-Methyl-2-a... mmmmnnm 58 6.40 6.60 6.80 7.00 m/z 59.10 8.61%

5000

30 41 15

/z—> 0 I'' I" " I ++l 72, I | I । I । |l । Il |ll । I | im p ' u|

5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 । | । ■ u | ■' ‘ । | । । " | I I I | । , ha... J 6.40 6.60 6.80 7.00

00831.D SCAN508.M Fri Feb 01 09:18:43 2002 Page 4

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