GCMS analysis results for sample AE00838, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN31\00831.D Vial: 4 Acq On : 31 Jan 2002 1:01 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************** * * * ** * ** * ** Peak Number 3 4H-1,2,4-Triazol-3-amine, 4.. Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

11.23 1.53 ug/L 666622 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4H-1,2,4-Triazol-3-amine, 4-prop... 126 C5H10N4 058661-97-5 47 2 Acetonitrile, (dimethylamino )- (... 84 C4H8N2 000926-64-7 43 3 Acetamide, N-formyl-N- [4-(1-form... 268 C13H20N2O4 054966-13-1 38 4 2 -Pyrrolidinemethanol, 1-methyl- 115 C6H13NO 003554-65-2 38 Abundance Scan 688 (11.229 min): 00831 .D (-) m/ z 84.05 100.00% 84 /

5000 42 126

98 141 i ■ 1 ■ ■ i ' 1 1 1 I ■ 1 ' 1 i 1 1 ' ' i ■ ■ 10.80 11.00 11.20 11.40 11.60 58 70 i m/z m/z-> 0 1 120 440 4 l 60 80 100 120 140 160 180 200 220 240 260 42.10 47.53% Abundance #22140: 4H-1,2,4-Triazol-3-amine, 4-propyl- (CAS) $$ 4H-1,.., 84

5000 97 TIr 126 T 10.80 11.00 11.20 11.40 11.60 43 55 70 m/z 126.10 46.20% 1 TTTT 01 -n-j-r-r-r-r-p n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #3157: Acetonitrile, (dimethylamino)- (CAS) $$ N.N-DIMETHY... 8|4

10.80 11.00 / 11.20 11.40 11.60 5000 m/z 44.10 20.37% 15 40 58 ।

m/z-> 01 —lI 11 20 40 1 1 ri 1 1 11 1 1 60 80 100 120 140 160 180 200 220 240 260 Abundance #210264: Acetamide, N-formyl-N-[4-(1-formyl-2-piperidinyl)... 84 10.80 11.00 11.20 11.40 11.60 m/z 98.10 18.33% 126 5000

43 56 96 205 221 265 0 —PT+ 011..... 1 I1 1 । i ' 1 ■ 1 1 1 T-r-r-T TT /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 10.80 11.00 11.20 11.40 11.60

30831.D SCAN508.M Fri Feb 01 09:18:43 2002 Page 5

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