GCMS analysis results for sample AE00838, Feb 2002

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Laboratory report showing GCMS analysis of sample AE00838 including surrogate recovery and unknown compounds.

NYC-WTC_000052187–000052204

Folder label: “GCMS X 1/11/02 A 1/31/02”

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NYC 9/11 Public Portal Document

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Data File : C:\MSDCHEM\1\5973N\02JAN31\00831.D Vial: 4 Acq On : 31 Jan 2002 1:01 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ************************************************* ** ****************** Peak Number 4 Tetradecane (CAS) $$ n-Tetr... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T.

16.86 0.52 ug/L 349764 Acenaphthene-dl0 18.34

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Tetradecane (CAS) $$ n-Tetradeca... 198 C14H30 000629-59-4 96 2 Tetradecane 198 C14H30 000629-59-4 95 3 Tetradecane (CAS) $$ n-Tetradeca... 198 C14H30 000629-59-4 93 4 Tetradecane (CAS) $$ n-Tetradeca... 198 C14H30 000629-59-4 91 Abundance Scan 1181 (16.857 min): 00831 .D (-) m/z 57.10 100.00% 57

43 71 5000 85

98 112 127 141 154 198 16.60 16.80 17.00 17.20

m/z—> 0 - 30 40 4— -ll NT , । FTThi । । | > 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 | I I II |’ I l r | . Ci । । I । I I | !> > i | I I ■ I | I I । TTTT m/z 43.10 61.96% Abundance #113303: Tetradecane (CAS) $$ n-Tetradecane $$ Isotetradecane 43 57 71 5000 85 16.60 16.80 17.00 17.20 m/ z 71.10 59.68%

m/z—> 0 m 99 113 127 141 154 198 1 1 ' । | । ' 1 I | 1,1 1 1 r" I'l I I H I |‘| i I । I ■ > ■ I I । I I I | . | . I | । I I | | I I I । I | I

30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #113289: Tetradecane 57 43 PPPPPPP 71 16.60 16.80 17.00 17.20 5000 85 m/ z 85.10 36.23%

Qo i 7 113 127 141 155 168 198 0 T" 111111111'11 r 1" TTTOTummmmn m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #113294: Tetradecane (CAS) $$ n-Tetradecane $$ Isotetradecane TIT "01 43 57 16.60 16.80 17.00 17.20 m/z 41.05 28.27% 71 5000 85

m/z—> 0 i" " r1 30 40 u TT 99 113 127 11'''11" il '1 rr’h "i111,111P111 gTn 1 TTTTT 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 141 155 198 111' 111' ।'' 11' । AA 1 PPTr । ' IUTTFpptr 16.60 16.80 17.00 17.20

00831.D SCAN508.M Fri Feb 01 09:18:43 2002 Page 6

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GCMS analysis results for sample AE00832, Feb 4 2002 · Box DEP Box 28

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