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GCMS analysis results for sample AE00838, Feb 2002

Machine-extracted title · confidence 90%

Laboratory report showing GCMS analysis of sample AE00838 including surrogate recovery and unknown compounds.

NYC-WTC_000052187–000052204

Folder label: “GCMS X 1/11/02 A 1/31/02

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Scanned page image, NYC-WTC_000052195
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN31\00831.D Vial: 4 Acq On : 31 Jan 2002 1:01 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 5 pentadecane Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

18.43 1.24 ug/L 835359 Acenaphthene-dl0 18 34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 pentadecane 212 C15H32 000629-62-9 97 2 Pentadecane 212 C15H32 000629-62-9 96 3 Pentadecane 212 C15H32 000629-62-9 96 4 Pentadecane 212 C15H32 000629-62-9 96 Abundance Scan 1319 (18.433 min): 00831.D (-) m/z 57.10 100.00%

43 57 I 71 5000- 85

18.00 18.20 18.40 18.60 18.80

m + 99 | 113 126 141 155 169 183 212 0 rrrTHTth 1 in fl1! 1 . | rrMiy I ! n ('l , I 11" I | ill f| 1 .11! 1 ' ' TTTTT m/ z 43.10 64.00% /z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #134049: pentadecane 57 43

71 _ v TTBBBmmu/m 5000 ■ 1 I ■ ■ 85 18.00 18.20 18.40 18.60 18.80 m/z 71.10 60.78% , 99 113 127 141 212 155 168 0 । ■■ ■11" " ।"111 TTT TITTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTT p rn p rrrp m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #134018: Pentadecane 57 43 ‘ I‘ ‘ ’ I’’ 18.00 18.20 18.40 18.60 18.80 5000 71 m/z85.10 40.97% 85

99 113 127 141 155 182 212 0 ’’’ ’1’11’4/1/11’1" - TTTLTTTTpm '1111 TTT m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #134012: Pentadecane - 1 -m Ppm n T 57 18.00 18.20 18.40 18.60 18.80 m/z 41.10 26.08% 71 5000 85

m/z—> 0 - m 99 । 113 127 141 155 169 TmmTDTTPmT 212 T..... T 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 200 210 (' " 1 I 1 ’I’T 18.00 18.20 18.40 18.60 18.80

30831 .D SCAN508.M Fri Feb 01 09:18:43 2002 Page 7

NYC-WTC_000052195

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NYC-WTC_000052195Source: NYC Law Department, mirrored locally

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