GCMS analysis results for sample AE00832, Feb 4 2002

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Laboratory report showing GCMS analysis of sample AE00832 including surrogate recovery and unknown compounds.

NYC-WTC_000052147–000052166

Folder label: “GCMS X 1/11/02 A 1/31/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN31\00832.D Vial: 5 Acq On : 31 Jan 2002 1:52 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 pentadecane Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 18.43 0.20 ug/L 168472 Acenaphthene-dl0 18.34 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 pentadecane 212 C15H32 000629-62-9 35 2 Undecane, 2,3-dimethyl- $$ 2,3-D... 184 C13H28 017312-77-5 35 3 Nonadecane $$ n-Nonadecane 268 C19H40 000629-92-5 35 4 Heptadecane 240 C17H36 000629-78-7 35 Abundance Scan 1319 (18.433 min): 00832.D (-) m/z 57.10 100.00% 57 43 71 5000 85 154

AAA—AA I , 98 113 127 18.00 18.20 18.40 18.60 18.80 0-T T’t ii I, I I1In!11! | 1"ill , I JI1 | | 1 7 I I | r I ii"I TTTTI m/z 71.10 62.51% /z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #134046: pentadecane 43 57

5000 71 ------- 18.00 18.20 18.40 18.60 18.80 85 m/z 43.10 60.10% 27 99 113 127 212 0 । ■ 1 1 r) < < I। < । 1 1 1 1 1 1 1 ■ ' I' l | » '■ ■ ■ I l-ri I | r I I I | 1 I l l | I I I !!!■!!! | I I I I | ! m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #93395: Undecane, 2,3-dimethyl- $$ 2,3-Dimethylundecane 43 57 71 MYMWh..a AW 18.00 18.20 18.40 18.60 18.80 5000 85 m/z 154.10 47.14%

27 140 — 99 111 0 TTur m/z-> :20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #211486: Nonadecane $$ n-Nonadecane v Tnnnnm [‘‘"‘I’’ 57 18.00 18.20 18.40 18.60 18.80 43 71 m/z 153.10 45.62% 85 5000

99 O-PPTTT 1113127 ............ 183 197.................. 268 " ■ | ■ 1 ■ > > I i ( । . > > । । i . > । । । r r ................ । i i r i । i i i i । i i i i । i I । i A TrT "I ' 1 I ■ ' /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 18.00 18.20 18.40 18.60 18.80

00832.D SCAN508.M Fri Feb 01 09:18:52 2002 Page 10

NYC-WTC_000052160

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NYC-WTC_000052160Source: NYC Law Department, mirrored locally

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GCMS analysis results for sample AE00839, Feb 4 2002 · Box DEP Box 28

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Laboratory report showing GCMS analysis of sample AE00839 including surrogate recovery and unknown compounds.

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