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GCMS analysis results for sample AE00832, Feb 4 2002

Machine-extracted title · confidence 90%

Laboratory report showing GCMS analysis of sample AE00832 including surrogate recovery and unknown compounds.

NYC-WTC_000052147–000052166

Folder label: “GCMS X 1/11/02 A 1/31/02

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Scanned page image, NYC-WTC_000052159
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN31\00832.D Vial: 5 Acq On : 31 Jan 2002 1:52 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************* * * **** * ***** Peak Number 7 Tetradecane (CAS) $$ n-Tetr... Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T. 16.87 0.15 ug/L 127755 Acenaphthene-dl0 18.34 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tetradecane (CAS) $$ n-Tetradeca... 198 C14H30 000629-59-4 95 2 Tetradecane 198 C14H30 000629-59-4 94 3 Tetradecane 198 C14H30 000629-59-4 93 4 Tetradecane (CAS) $$ n-Tetradeca... 198 C14H30 000629-59-4 93 Abundance Scan 1182 (16.868 min): 00832. D (-) m/ z 57.10 100.00% 57 43 71 5000 85

99 A/ । । I f । i i i r । I i I rrroT"I‘I । । 16.60 16.80 17.00 17.20

n/z-> 0 —lll — TI’T V-mm 112 126 141150 | 198 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 TTTTTTLTTTTTTTTTTTTT m/z 43.10 63.08%

Abundance #113293: Tetradecane (CAS) $$ n-Tetradecane $$ Isotetradecane 57 71 5000 85 1 ' i ' A 16.60 16.80 17.00 17.20 m/z 71.10 58.27% 99 113 127 141 155 168 198 o । ■■ ■ ■ ।) — PTmm)ummu m mlz-> 30 40 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #113299: Tetradecane 57 71 A I V A A TnEDOnTT 85 16.60 16.80 17.00 17.20 5000 m/ Z 85.10 39.68%

OTTTTTTTT TT’T 113127141 419 UTT1i i । if i I । । । । । । li । ■ । ‘ ‘‘ । 11 ri । i i i I | ! I ‘ I pin I IT ITTTETTEri | I nt m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance 57 #113289: Tetradecane /A A 16.60 16.80 17.00 17.20 43 m/ Z 41.10 35.11% 71 5000 85

QQ

m/z-> 0— 30 40 . 7 113 TTTUTETTm)TTTDnu 127 141 155 168 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 198 AAMLWAAAA 16.60 16.80 17.00 17.20

00832.D SCAN508.M Fri Feb 01 09:18:52 2002 Page 9

NYC-WTC_000052159

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NYC-WTC_000052159Source: NYC Law Department, mirrored locally

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