GCMS analysis results for sample AE00832, Feb 4 2002

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Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN31\00832.D Vial: 5 Acq On : 31 Jan 2002 1:52 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 Tridecane Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 15.19 0.30 ug/L 239228 Naphthalene-d8 13.19 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Tridecane 184 C13H28 000629-50-5 95 2 Tridecane 184 C13H28 000629-50-5 92 3 Tridecane (CAS) $$ n-Tridecane $... 184 C13H28 000629-50-5 90 4 Heptadecane 240 C17H36 000629-78-7 90 Abundance Scan 1035 (15.190 min): 00832.D (-) "2 57.05 100.00% 57 43 71 5000 85 mmmm m/z-> Abundance 01 20 mmTi 30 40 uH 50 h 99 112 126 141 184 ------- 1111'1'111' ■ ■ ir''11111 ■ r 111111 60 70 80 90 100 110 120 130 140 150 160 170 180 190 14.80 15.00 15.20 15.40 15.60 m/ Z 43. 10 63.57% #93367: Tridecane 57 43

71 5000 85 14.80 15.00 15.20 15.40 15.60 m/ z 71. 10 58.31% 0 ■ i'1 r' ir 1'' I' — . 99 113 127 141 155 1111—unB—uwnT—him TTT* f | > < > I | > I . I | I’l I I | I I I1! | 184 1 mlz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #93364: Tridecane 43 57 A , 11 110 . / in MT r । ■ > 71 14 80 15.00 15.20 15.40 15.60 5000 85 m/z 85.10 36.46%

f 112 127 141 184 0 - ‘ 11111 UTT TItt TTTTTTTTTTTTTTu m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #93376: Tridecane (CAS) $$ n-Tridecane $$ Tridecane, n- 43 57 14.80 15.00 15.20 15.40 15.60 m/ Z 41.10 29.33% 5000

O-TTTT 27 J 1 ITl’ TOrr 71

99 112 127 TTTTUTTUT l 85

184 Tmpu 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 □ PM 14.80 15.00 15.20 15.40 15.60

10832.D SCAN508.M Fri Feb 01 09:18:52 2002 Page 8

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