GCMS analysis results for sample AE00466, Jan 18 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C : \MSDCHEM\1\5973N\02JAN10\00473 . D Vial: 8 Acq On 10 Jan 2002 8:36 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 Tridecane Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 22.05 0.33 ug/L 196935 Phenanthrene -dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tridecane 184 C13H28 000629-50-5 64 2 Pentacosane $$ n-Pentacosane 352 C25H52 000629-99-2 59 3 Tridecane (CAS) $$ n-Tridecane $... 184 C13H28 000629-50-5 58 4 Triacontane$$n-Triacontane 422 C30H62 000638-68-6 53 Abundance Scan 1636 (22.052 min): 00473.D (-) m/z 57.10 100.00% 57

5000

4 85 ALp 21.80 22.00 22.20 22.40 0- TTTrr —74 10107’23 141.1.169184 213 229 250 i ■'1 ■ i1' ■ ■ i ■' ■ ■ i' ■ ■ ■ i m/z 71.10 57.52% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #93367: Tridecane 57

5000 85 21.80 22.00 22.'20 22.40 m/z 85.10 45.80% J60 80i 100- 113120 140 No 184 141 TVunuuuuuunaUTpTip Oui) T’T । r ml 11 111* 11 m/z-> 40 160 180 200 220 240 260 280 300 320 340 Abundance #300501: Pentacosane $$ n-Pentacosane 57

21.80 22.00 22.20 22.40 5000 85 m/z 43.10 45.20%

0 , .1 113 141 । 169 196 TTT , 4 1 TTTO11uuuuTTT J 281296 352 TTTu’Outui p/ miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #93370: Tridecane (CAS) $$ n-Tridecane $$ Tridecane, n- 57 21.80 22.00 22.20 22.40 m/ z 69.10 22.76% 5000 85

, , 113 141 184 0 ■■i' ■ ■11'1 - 1’’ ' * I m/z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 21.80 22.00 22.20 22.40

30473.D SCAN508.M Fri Jan 11 10:09:09 2002 Page 6

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