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GCMS analysis results for sample AE00249, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report listing unknown compounds and surrogate recovery for sample AE00249 analyzed on January 28, 2002.

NYC-WTC_000050577–000050595

Folder label: “GCMS X 1/4/02 A 1/24 - 1/25/02

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Scanned page image, NYC-WTC_000050594
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C: \MSDCHEM\1\5973N\02JAN24\00249.D Vial: 5 Acq On : 24 Jan 2002 6:17 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 24’, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library- : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 Tritriacontane (CAS) $$ n-T... Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

36.61 0.13 ug/L 77138 Perylene-dl2 34.42

Hit# of 5 Tentative ID MW Mol Form • CAS# Qual 1 Tritriacontane (CAS) $$ n-Tritri... 465 C33H68 000630-05-7 72 2 Hexatriacontane 507 C36H74 000630-06-8 72 3 Triacontane 422 C30H62 000638-68-6 72 4 Octacosane_____ 394 C28H58 000630-02-4 72 Abundance Scan 2911 (36.608 min): 00249. D (-) m/z 57.10 100.00%| 57 - 85

5000-

36.20 36.40 36.60 36.80 37.00 .1 1 1 1 ‘ 1 1 1 1 ' 208 m/z 71.10 97.15%

l ‘ • i 1 I 1 1 1 ' t ■ ■ ■ • i ■ ■ ‘ ■ i ■ 1 • ■ i 1 1 ' ' i 1 mz-> 50 100 150 200 250 300 350 400 450 Abundance #359682: Tritriacontane (CAS) $$ n-Tritriacontane 57

5000- 85 NWW)MV 36.20 36.40 36.60 36.80 37.00 43.10 78.52%

L m/z

■ ■ 1‘" 1 111 169 281 309 337 379 407 435 464 miz-> 50 100 150 200 250 300 350 400 450 Abundance #369892: Hexatriacontane 57

36.20 36.40 36.60 36.80 37.00 5000 m/z 85.10 68.66% 85

‘ ■ i ■ I 1113.141169. 197. miz-> Abundance 43 50 100 150 200 250 ‘300 #343922: Triacontane 350 ‘400' 450' WM1 A 1 • i1 ■ 36.20 36.40 36.60 36.80 37.00 m/z 55.10 37.63% 71 5000

• ' । ■ 12,177 |.... . 239 267 *(**14***1 379 422 /z—> 50 100 150 200 250 300 350 400 450 36.20 36.40 36.60 36.80 37.00

00249.D SCAN508.M Fri Jan 25 10:26:18 2002 Page 14

NYC-WTC_000050594

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NYC-WTC_000050594Source: NYC Law Department, mirrored locally

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