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GCMS analysis results for sample AE00249, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report listing unknown compounds and surrogate recovery for sample AE00249 analyzed on January 28, 2002.

NYC-WTC_000050577–000050595

Folder label: “GCMS X 1/4/02 A 1/24 - 1/25/02

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NYC 9/11 Public Portal Document

Library Search Compound Report • Data File : C:\MSDCHEM\1\5973N\02JAN24\00249.D Vial: 5 Acq On : 24 Jan 2002 6:17 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 Tetratriacontane $$ n-Tetra... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 34.12 0.45 ug/L 272621 Perylene-dl2 34.42 Hit# of 5 Tentative ID MW MolForm . CAS# Qual 1 Tetratriacontane $$ n-Tetratriac... 479 C34H70 014167-59-0 90 2 Tricosane (CAS) $$ n-Tricosane 324 C23H48 000638-67-5 87 3 Docosane $$ n-Docosane $$ Normal... 310 C22H46 000629-97-0 87 4 Heneicosane $$ n-Heneicosane 296 C21H44 000629-94-7 87 Abundance Scan 2693 (34.119 min): 00249.D (-) m/z 57.10 100.00% 57

85 5000

33,80 34.00 34.20 34.40 207 nz-> TTI T 1, 1113, 141169 Tp |T, ’ ’111’144 pj-n, 11, if 40 60 80 100120140160180200 220240260280300320340360380400 m/z 71.10 66.91% Abundance #363627: Tetratriacontane $$ n-Tetratriacontane 57

A A/wAA / 5000 85 33.80 34.00 34.20 34.40 m/z 85.10 57.35%

• ■ i ■1 ■ 1.17134141, 169 1’111-011000011010133311317517 1.111,11।1, ।।1, ,1. 311 1, 367 410 1.... । n/z-> 40 60 80 100 120140160180200220240260280300320340360380400 Abundance #275685: Tricosane (CAS) $$ n-Tricosane 57 A ’AII /_______ Aa । . » I .IT. j rr 33.80 34.00 34.20 34.40 AMA 50001 85 m/z43.10 50.45%

111 111 ....................................................................................... ............ ^-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400

u Abundance #261311: Docosane $$ n-Docosane $$ Normal-docosane 57 33.80 34.00 34'20 34.40 m/ z 55.10 22.45% 85 5000

, 113 . -rrp-r 1141 ,169 266 310 1 1 1 I । 1 1 H । 1 1 t 1 । 1 < 1 > । 1 > > I । i t > 1 | > 1 I 1 । 1 • 1 1 | 1 1 > i j « /1 • । 1 ■ 1 1 | 1 1 ■ > । • 1 t ■ | 1 > • 1 | TT nz—> 40 60 80 100120140160180200220240260280300320340360380400 33.80 34.00 34.20 34.40

00249.D SCAN508.M Fri Jan 25 10:26:17 2002 Page 11

NYC-WTC_000050591

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