GCMS analysis results for sample AE00249, Jan 2002

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Laboratory report listing unknown compounds and surrogate recovery for sample AE00249 analyzed on January 28, 2002.

NYC-WTC_000050577–000050595

Folder label: “GCMS X 1/4/02 A 1/24 - 1/25/02”

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NYC 9/11 Public Portal Document Library Search Compound Report , Data File : C: \MSDCHEM\ 1\597302JAN2 4\00249.D Vial: 5 Acq On : 24 Jan 2002 6:17 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 Tetratriacontane $$ n-Tetra... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T.

33.26 0.24 ug/L 141987 Perylene-dl2 34.42

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Tetratriacontane $$ n-Tetratriac... 479 C34H70 014167-59-0 90 2 Heneicosane $$ n-Heneicosane 296 C21H44 000629-94-7 87 3 Docosane, 11-decyl- (CAS) $$ 11-... 451 C32H66 055401-55-3 86 4 Tetratetracontane $$ n-Tetratetr... 619 C44H90 007098-22-8 83 Abundance Scan 2618 (33.263 min): 00249.D (-) m/z 57.10 100.00% 57

85 5000 AMAA 1 ■R T 207 33.00 33.20 33.40 33.60 I l ll 1 11 Mihi 113। T‘1410uuu—mBn——1 2m—n—m“mnmmana m/z 71.10 73.63% n/z-> 40 60 80 100120140160180200220240260280300320 340 360380400 Abundance #363627: Tetratriacontane $$ n-Tetratriacontane 57

5000 85 -AA-A-PA 33.00 33.20 33.40 33.60 m/z43.10 57.58%

miz-> “ i" ■ 1.11134141 169 311 1′00111111011110100111911901111110211377112217112111100710771077711 40 60 80 100120140160180200 220240260280300320340360380400 367 410

Abundance #245745: Heneicosane $$ n-Heneicosane 57 ‘ ■ i ■ ■ ■ ■ i 1 ' 33.00 33.20 33.40 33.60 85 5000 m/z 85.10 52.86%

.................................................... "i"' ,. .1.1′4. i(< < r11 ■ > > > f> । ................................ 11 < > > 111 > > j > > < >। > > > > j i) > >] । ■ >11111111 > < > 111 ■ 11 ■ ■ h j 11...... >111 ■ >....... >(> > < >। niz-> 40 60 80 100120140160180200220240260280300320340360380400 Abundance #355038: Docosane, 11-decyl- (CAS) $$ 11-n-Decyldocosane $... i « । i i i t | ‘i i i i’P’ ’ ‘ ’ i ‘ ' 14 57 33.00 33.20 33.40 33.60 m/z 83.10 20.13% 5000 85

_113.14116919725 T‘10011300000r21""T —Bu-B—0-B——BI0-EUU‘m"‘IE"09311B1—3-19U0-0U—3W"I‘‘I—C—OW—TI0-EIT 33.00 33.20 33.40 33.60 mfz~> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400

00249.D SCAN508.M Fri Jan 25 10:26:17 2002 Page 10

NYC-WTC_000050590

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