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GCMS analysis results for sample AE00249, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report listing unknown compounds and surrogate recovery for sample AE00249 analyzed on January 28, 2002.

NYC-WTC_000050577–000050595

Folder label: “GCMS X 1/4/02 A 1/24 - 1/25/02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN24\00249.D Vial: 5 Acq Oh : 24 Jan 2002 6:17 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 Octadecane, 2,2,4,15,17,17-... Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

32.38 0.10 ug/L 69469 Chrysene-dl2 30.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Octadecane, 2,2,4,15,17,17-hexam... 591 C42H86 055470-97-8 53 2 Octadecane, 2,2,4,15,17,17-hexam... 591 C42H86 055470-97-8 53 3 Docosane (CAS) $$ n-Docosane $$ ... 310 C22H46 000629-97-0 47 4 dihexyl sulfide______________________ 202 C12H26S 000000-00-0 28 Abundance Scan 2541 (32.384 min): 00249. D (-) m/z 57.10 100.00% 57

5000 85 AAW 32.00 32.20 32.40 32.60 32.80 • l • m/z 43.10 66.34% nz-> 50 100 150 200 250 300 350 400 450 500 Abundance #381124: Octadecane, 2,2,4,15,17,17-hexamethyl-7,12-bis(3,... 57

5000 m 32.00 3220 3240 32.60 32.80 m/z 71.10 60.20% j 85 113 141 169 211 —’1*eh**1*** 534 ’I’*’’I**II1| niz-> 50 100 150 200 250 300 350 400 450 500 Abundance #381123: Octadecane, 2,2,4,15,17,17-hexamethyl-7,12-bis(3,... 57 .......1.,MW 32.00 32.20 32.40 32.60 32.80 5000 m/z 85.10 46.72%

— , 85.113 141 169 211 ................................. mz—> 50 100 150 200 250 300 350 400 450 500 Abundance #261318: Docosane (CAS) $$ n-Docosane $$ C22H46 STANDARD $... 57 32.00 32.20 '3240' 32.60 32.80 m/z 55.10 36.11%

5000 85

' 1 1 miz—> 50 100 ’150 200 250 300 350 ’400 450 500" 32.00 32.20 3240 32.60 32.80

00249.D SCAN508.M Fri Jan 25 10:26:17 2002 Page 9

NYC-WTC_000050589

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NYC-WTC_000050589Source: NYC Law Department, mirrored locally

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