GCMS surrogate recovery results, sample AE07110, April 15, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File : C:\MSDCHEM\l\DATA\041002\7110.D Vial: 17 Acq On : 11 Apr 2002 3:12 am Operator: Bohlk Sample : SAMPLE 7110 3/27/02 Inst : Instrumen Mise . : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peale Number 12 Nonadecane Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

29.49 21.58 ug/L 2590100 Chrysene-dl2 30.14 .

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Nonadecane 268 C19H40 000629-92-5 91 2 Docosane $$ n-Docosane $$ Normal... 310 C22H46 000629-97-0 91 3 Eicosane 282 C20H42 000112-95-8 91 4 Heptacosane _____________________________ 380 C27H56 _____ 000593-49-7 90 Abundance Scan 4495 (29.490 min): 7110.D (-) m/z 57.10 100.00% 5Z

5000 85

m/z-> Abundance OV Mih ^39 267 295 TTTrjrtTTpTTVp-fTT-pTTTpTTTTTTTrpTTTJT^^ 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #211478; Nonadecane ■ 338 m/z 29.20 29.40 29.60 29.80 71.10 58.76%

7

5000 85 II 29.20 29.40 29.60 29.80 m/z 43.10 44.91%

OV m/z-> 20 40 60 80 100120140160180 200 220 240 260 280 300 320 340 Abundance #261311; Docosane $$ n-Docosane $$ Normai-docosane 57

85 29.20 29.40 29.60 29.80 Wilil m/z 85.10 43.15%

0 11.. q. .7.1 n MI. I n I. r.. I.... I.... 11.. .'I. I. I... (.... I.. I m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #228992: Eicosane 57 29.20 29.40 29.60 29.80 m/z 55.10 22.35%

5000 85 29 I ,I' ■p* J|T. 1 qJ IT 0 I''" J41 169 iT, I I'l i i f 11 n 11 n 11 282 I' •" 1.1 ■ •n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 I 29.20 29.40 29.60 29.80

'110.D 5080402BB.M Mon Apr 15 17:09:22 2002 Page 14

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