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GCMS sample AE07115 results, April 25, 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry analysis results for sample AE07115 including detection of unknown compounds.

NYC-WTC_000049063–000049101

Folder label: “GCMS X 4/12/02 A 4/23/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\041002\7115.D Vial: 22 Acq On : 11 Apr 2002 7:15 am Operator: Bohik Sample : SAMPLE 7115 3/27/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 6 Docosane (CAS) $$ n-Docosan... Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

27.38 48.61 ug/L 5952230 Chrysene-dl2 30.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Docosane (CAS) $$ n-Docosane $$ ... 310 C22H46 000629-97-0 97 2 Docosane 310 C22H46 000629-97-0 95 3 Nonadecane (CAS) $$ n-Nonadecane 268 C19H40 000629-92-5 91 4 Heneicosane $$ n-Heneicosane 296 C21H44 000629-94-7 90 Abundance Scan 4136 (27.381 min): 7115.D (-) m/z 57.10 100.00% 57

5000 85 -JV__________ 4 27.66 27.20 27.40 27.60 27.80 0 TI +A..113.141,,168,197,,225.253.281..310, m/z 71.10 56.09% miz—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance#261317: Docosane (CAS) $3 n-Docosane SS C22H46 STANDARD 3... 57

85 5000 11,1' KITT ....... 1.... 1. i 27.00 27.20 27.40 27.60 27.80 m/z 43.15 42.49% l 113 4A4 11. 141 169 197 310 1 0 "15-31111111211011711101133320711117 miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #261313: Docosane 57

T T T T 27.00 27.20 27.40 27.60 27.80 5000 85 m/z 85.15 39.80%

4' I । 141

m/z-> 0— pikkum44+■ 4 167183, ,211,239, .267., ■. ■ ■ 310, 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #211483: Nonadecane (CAS) $$ n-Nonadecane 57 27.00 27.20 27.40 27*60 27.80 m/z 55.10 19.83%

5000 85

0-por 111188,197..225.R It T T T‘3 m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 27.00 27.20 27.40 27.60 27.80

7115.D 5080402BBC.M Tue Apr 23 15:52:54 2002 Page 9

NYC-WTC_000049086

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NYC-WTC_000049086Source: NYC Law Department, mirrored locally

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