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GCMS sample AE07115 results, April 25, 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry analysis results for sample AE07115 including detection of unknown compounds.

NYC-WTC_000049063–000049101

Folder label: “GCMS X 4/12/02 A 4/23/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\041002\7115.D Vial: 22 Acq On : 11 Apr 2002 7:15 am Operator: Bohik Sample : SAMPLE 7115 3/27/02 Inst : Instrumen Mise Multipir: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 5 Heneicosane Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

26.25 25.08 ug/L 3070520 Chrysene-dl2 30.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Heneicosane 296 C21H44 000629-94-7 95 2 Iron, tricarbonyl[N-(phenyl-2-py... 398 C21H14FeN2O3 074764-11-7 91 3 Nonadecane (CAS) $$ n-Nonadecane 268 C19H40 000629-92-5 91 4 Eicosane 282 C20H42 000112-95-8 91 Abundance Scan 3943 (26.247 min): 7115.D (-) m/z 57.10 100.00% 57

5000

41 85 J 1111**0* 26.00 26.20 26.40 26.60

m/z-> 0 -...‘1+141..168,197—725,253— 20 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 m/z 71.10 58.91%

Abundance #245744: Heneicosane 57

5000 85 26.00 26'20 26.40 26.60 4I m/z 43.15 44.78%

44 113 1 i 111 169 211 239 Ol TLTTTT ip .q I r|* ufri A r h puifpe n 11 h . .'i 11 r ■ 267 i n' ■ i ■' ‘h' m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #331028: Iron, tricarbonyl[N-(phenyl-2-pyridinylmethylene)... 57

26.00 26.20 26.40 26.60 m/z 85.15 39.23% 5000 85

41

m/z-> 0 2244ITi 113rfriJ 141■ hi rm , 169 . 197 225 253 282 i fi ntpi)! 11".. q ■ ■ ■ ■ 111 ■. ... |. 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #211483: Nonadecane (CAS) $$ n-Nonadecane 57 T T T T 26.00 26.20 26.40 26.60 m/z 55.10 20.80%

5000 85

0 .3141162/19725/268, m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 26.00 26.20 26.40 26.60

7115.D 5080402BBC.M Tue Apr 23 15:52:53 2002 Page 8

NYC-WTC_000049085

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NYC-WTC_000049085Source: NYC Law Department, mirrored locally

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